Fourier transform infrared spectrometry
著者
書誌事項
Fourier transform infrared spectrometry
(Chemical analysis, v. 171)
John Wiley & Sons, Inc., c2007
2nd ed
大学図書館所蔵 全9件
  青森
  岩手
  宮城
  秋田
  山形
  福島
  茨城
  栃木
  群馬
  埼玉
  千葉
  東京
  神奈川
  新潟
  富山
  石川
  福井
  山梨
  長野
  岐阜
  静岡
  愛知
  三重
  滋賀
  京都
  大阪
  兵庫
  奈良
  和歌山
  鳥取
  島根
  岡山
  広島
  山口
  徳島
  香川
  愛媛
  高知
  福岡
  佐賀
  長崎
  熊本
  大分
  宮崎
  鹿児島
  沖縄
  韓国
  中国
  タイ
  イギリス
  ドイツ
  スイス
  フランス
  ベルギー
  オランダ
  スウェーデン
  ノルウェー
  アメリカ
内容説明・目次
内容説明
A bestselling classic reference, now expanded and updated to cover the latest instrumentation, methods, and applications
The Second Edition of Fourier Transform Infrared Spectrometry brings this core reference up to date on the uses of FT-IR spectrometers today. The book starts with an in-depth description of the theory and current instrumentation of FT-IR spectrometry, with full chapters devoted to signal-to-noise ratio and photometric accuracy. Many diverse types of sampling techniques and data processing routines, most of which can be performed on even the less expensive instruments, are then described. Extensively updated, the Second Edition:
*
Discusses improvements in optical components
*
Features a full chapter on FT Raman Spectrometry
*
Contains new chapters that focus on different ways of measuring spectra by FT-IR spectrometry, including fourteen chapters on such techniques as microspectroscopy, internal and external reflection, and emission and photoacoustic spectrometry
*
Includes a new chapter introducing the theory of vibrational spectrometry
*
Organizes material according to sampling techniques
Designed to help practitioners using FT-IR capitalize on the plethora of techniques for modern FT-IR spectrometry and plan their experimental procedures correctly, this is a practical, hands-on reference for chemists and analysts. It's also a great resource for students who need to understand the theory, instrumentation, and applications of FT-IR.
目次
PREFACE. CHAPTER 1. INTRODUCTION TO VIBRATIONAL SPECTROSCOPY.
1.1. Introduction.
1.2. Molecular Vibrations.
1.3. Vibration-Rotation Spectroscopy.
1.4. Widths of Bands and Lines in Infrared Spectra.
1.5. Quantitative Considerations.
1.6. Polarized Radiation.
1.7. Raman Spectrometry.
1.8. Summary.
CHAPTER 2 THEORETICAL BACKGROUND.
2.1. Michelson Interferometer.
2.2. Generation of an Interferogram.
2.3. Effect of Finite Resolution.
2.4. Apodization.
2.5. Phase Effects.
2.6. Effect of Beam Divergence.
2.7. Effect of Mirror Misalignment.
2.8. Effect of a Poor Mirror Drive.
2.9. Rapid-Scan Interferometers.
2.10. Step-Scan Interferometers.
CHAPTER 3 SAMPLING THE INTERFEROGRAM.
3.1. Sampling Frequency.
3.2. Aliasing.
3.3. Dynamic Range.
3.4. Analog-to-Digital Converters.
CHAPTER 4 FOURIER TRANSFORMS.
4.1. Classical Fourier Transform.
4.2. Fast Fourier Transform.
4.3. Phase Correction.
4.4. Fourier Transform: Pictorial Essay.
4.5. Data Systems.
CHAPTER 5 TWO-BEAM INTERFEROMETERS.
5.1. Michelson-Type Interferometers.
5.2. Tilt-Compensated Interferometers.
5.3. Refractively Scanned Interferometers.
5.4. Polarization Interferometers.
5.5. Step-Scan Interferometers.
5.6. Stationary Interferometers.
5.7. Beamsplitters.
5.8. Lamellar Grating Interferometers.
Appendix: Manufacturers of FT-IR Spectrometers.
CHAPTER 6 OTHER COMPONENTS OF FT-IR SPECTROMETERS.
6.1. Infrared Radiation Sources for Transmission and Reflection Spectrometry.
6.2. Detectors.
6.3. Optics.
6.4. Spectrometer Design.
CHAPTER 7 SIGNAL-TO-NOISE RATIO.
7.1. Detector Noise.
7.2. Trading Rules in FT-IR Spectrometry.
7.3. Digitization Noise.
7.4. Other Sources of Noise.
7.5. Interferometers Versus Grating Spectrometers.
CHAPTER 8 PHOTOMETRIC ACCURACY IN FT-IR SPECTROMETRY.
8.1. Introduction.
8.2. Effect of Spectral Resolution.
8.3. Effect of Apodization.
8.4. 100% Lines.
8.5. Zero Energy Level.
8.6. Linearity Between 100% and 0%T.
CHAPTER 9 QUANTITATIVE ANALYSIS.
9.1. Introduction.
9.2. Beer's Law.
9.3. Spectral Subtraction.
9.4. Linear Least-Squares Fitting Methods.
9.5. Classical Least Squares.
9.6. Inverse Least-Squares Regression.
9.7. Principal Component Analysis.
9.8. Principal Component Regression.
9.9. Partial Least-Squares Regression.
9.10. Validation.
9.11. Multivariate Curve Resolution.
9.12. General Guidelines for Calibration Data Sets.
9.13. Neural Networks.
CHAPTER 10 DATA PROCESSING.
10.1. Baseline Correction.
10.2. Interpolation.
10.3. Peak Picking.
10.4. Spectral Smoothing.
10.5. Band Fitting.
10.6. Derivatives of Spectra.
10.7. Fourier Self-Deconvolution.
10.8. Spectral Searching.
CHAPTER 11 CONVENTIONAL TRANSMISSION SPECTROMETRY.
11.1. Condensed-Phase Samples.
11.1.4 Trace Analysis.
11.2. Gas- and Vapor-Phase Samples.
CHAPTER 12 POLARIZATION.
12.1. Plane-Polarized Radiation.
12.2. Circular Polarization.
12.3. Polarization Modulation.
12.4. Applications of Linear Dichroism.
12.5. Vibrational Circular Dichroism.
CHAPTER 13 SPECULAR REFLECTION.
13.1. Introduction.
13.2. Fresnel Reflection from Bulk Samples.
13.3. Infrared Reflection-Absorption Spectrometry with Metal Substrates.
13.4. IRRAS with Dielectric Substrates.
13.5. Transflection.
13.6. Summary.
CHAPTER 14 MICROSPECTROSCOPY AND IMAGING.
14.1. Microsampling with Beam Condensers.
14.2. Microscopes.
14.3. Diamond Anvil Cells.
14.4. Reflection Microscopy.
14.5. Hyperspectral FT-IR Imaging.
CHAPTER 15 ATTENUATED TOTAL REFLECTION.
15.1. Introduction.
15.2. Theory.
15.3. Practical Considerations.
15.4. Accessories for Multiple Internal Reflection.
15.5. Single-Reflection Accessories.
15.6. Infrared Fibers.
15.7. Summary.
CHAPTER 16 DIFFUSE REFLECTION.
16.1. Theory of Diffuse Reflection.
16.2. Accessories for Diffuse Reflection.
16.3. Applications of Mid-Infrared Diffuse Reflection Spectrometry.
16.4. Applications of Near-Infrared Diffuse Reflection Spectrometry.
16.5. Reference Materials for Diffuse Reflection Spectrometry.
CHAPTER 17 EMISSION.
17.1. Introduction.
17.2. Infrared Emission Spectra of Gases.
17.3. Infrared Emission Spectra of Condensed-Phase Samples.
17.4. Transient Infrared Emission Spectroscopy.
CHAPTER 18 FOURIER TRANSFORM RAMAN SPECTROMETRY.
18.1. Introduction.
18.2. Instrumentation.
18.3. FT Raman Versus CCD Raman Spectrometry.
18.4. Applications of FT-Raman Spectrometry.
18.5. Summary.
CHAPTER 19 TIME-RESOLVED SPECTROMETRY.
19.1. Continuous-Scanning Interferometers.
19.2. Time-Resolved Measurements Using Step-Scan Interferometers.
19.3. Stroboscopic Spectrometry.
19.4. Asynchronous Time-Resolved FT-IR Spectrometry.
CHAPTER 20 PHOTOACOUSTIC SPECTROMETRY.
20.1. Photoacoustic Spectroscopy of Gases.
20.2. Photoacoustic Spectroscopy of Solids with a Rapid-Scanning Interferometer.
20.3. Photoacoustic Spectroscopy of Solids with a Step-Scan Interferometer.
CHAPTER 21 SAMPLE MODULATION SPECTROMETRY WITH A STEP-SCAN INTERFEROMETER.
21.1. Dynamic Infrared Linear Dichroism Measured with a Monochromator.
21.2. DIRLD Spectrometry with a Step-Scan Fourier Transform Spectrometer.
21.3. Two-Dimensional Correlation Plots.
21.4. DIRLD Spectrometry with a FT-IR Spectrometery and Digital Signal Processing.
21.5. Other Sample Modulation Measurements with Step-Scan Interferometers.
CHAPTER 22 ATMOSPHERIC MONITORING.
22.1. Extractive Atmospheric Monitoring.
22.2. Open-Path Atmospheric Monitoring.
CHAPTER 23 COUPLED TECHNIQUES.
23.1. Introduction.
23.2. Light-Pipe-Based GC/FT-IR Interfaces.
23.3. Mobile-Phase Elimination Approaches for GC/FT-IR.
23.4. HPLC/FT-IR Interface.
23.5. SFC/FT-IR Interface.
23.6. TGA/FT-IR.
23.7. Other Coupled Techniques.
INDEX.
「Nielsen BookData」 より