Techniques in organic chemistry : miniscale, standard taper microscale, and Williamson microscale
著者
書誌事項
Techniques in organic chemistry : miniscale, standard taper microscale, and Williamson microscale
W.H. Freeman, c2010
3rd ed
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注記
Includes index
内容説明・目次
内容説明
Techniques in Organic Chemistry is the most comprehensive and detailed presentation of lab techniques available for organic chemistry students - and the least expensive. It combines specific instructions for 3 different kinds of laboratory glassware (miniscale,standard-taper microscale, )Williamson microscale) and offers extensive coverage of spectroscopic techniques, and a strong emphasis on safety issues. The techniques manual can be packaged with either version of Mohrig, Modern Projects and Experiments in Organic Chemistry, with an instructor's own experiments through Freeman Custom Publishing, or may be purchased separately.
目次
PART I: INTRODUCTION TO THE ORGANIC LABORATORY ESSAY: The Role of the Laboratory Safety in the Laboratory Protecting the Environment Laboratory Notebooks and Prelaboratory Information PART II: CARRYING OUT CHEMICAL REACTIONS ESSAY: Learning to Do Organic Chemistry Laboratory Glassware Measurements and Transferring Reagents Heating and Cooling Methods Assembling a Reaction Apparatus Computational Chemistry Planning a Chemical Reaction PART III: SEPARATION AND PURIFICATION TECHNIQUES ESSAY: Intermolecular Forces in Organic Chemistry Filtration Extraction Drying Organic Liquids and Recovering Reaction Products Boiling Points and Distillation Melting Points and Melting Ranges Recrystallization Specialized Techniques PART IV: CHROMOTOGRAPHIC SEPARATION AND ANALYSES ESSAY: Modern Chromatographic Separations Thin-Layer Chromatography Liquid Chromotography Gas-Liquid Chromotography PART V: SPECTROSCOPIC METHODS ESSAY: The Spectroscopic Revolution Infrared Spectroscopy 1H Nuclear Magnetic Resonance Spectroscopy 13C and Two-Dimensional NMR Spectroscopy Mass Spectrometry Ultraviolet and Visible Spectroscopy Integrated Spectroscopy Problems
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