The use of electrochemical scanning tunnelling microscopy (EC-STM) in corrosion analysis : reference material and procedural guidelines
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Bibliographic Information
The use of electrochemical scanning tunnelling microscopy (EC-STM) in corrosion analysis : reference material and procedural guidelines
（European Federation of Corrosion publications, no. 44）（Woodhead publishing in materials）
Woodhead Publishing , CRC Press, 2007
- : Woodhead Pub.
- : CRC Press
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Published for the European Federation of Corrosion by Woodhead Publishing and Maney Publishing on behalf of Institute of Materials, Minerals & Mining --- t.p.
Includes bibliographical references
Description and Table of Contents
- Volume
-
: CRC Press ISBN 9781420051193
Description
The use of EC-STM to study the relationship between surface structure and surface reactivity in situ on electrodes in contact with an electrolyte is of major importance in corrosion research. Highlighting this essential topic in corrosion science, this book supplies the reference material and procedural guidelines required for the application of electrochemical scanning tunnelling microscopy (EC-STM). STM-users are instructed how to obtain high resolution data on a carefully prepared copper single-crystal surface. After reviewing the background of the copper system, the book covers experimental design, moire pattern formation on Cu, and problems with imaging.
Table of Contents
INTRODUCTION
Background to the Copper System Experimental Description
Surface preparation: Mechanical polishing, Electropolishing, Annealing
Experiment preparation: Preparation of solutions, Preparation of tips, Cleaning the cell
Setting the microscope: Mounting the head and adjusting the height
Setting the cell and adding electrolyte
Running the microscope: Tip approach, Imaging, Electrochemistry, Tip withdrawal
Moire Pattern Formation on Cu (111)
Cyclic voltammetry
Imaging at fixed potential
Sweeping the potential during imaging
Problems with Imaging
Instability and drift
Poorly resolved images
References
- Volume
-
: Woodhead Pub. ISBN 9781845692353
Description
The European Federation of Corrosion's Working Party on Surface Science and the Mechanisms of Corrosion and Protection (EFC WP6) has defined, as one of its objectives, the development of a reference material and reference guidelines for the application of electrochemical scanning tunnelling microscopy (EC-STM) in corrosion science. The use of EC-STM to study the relationship between surface structure and surface reactivity in situ on electrodes in contact with an electrolyte is of major importance in corrosion research. This report describes the reference material and procedural guidelines required to use this technique effectively. STM-users are instructed how to obtain high resolution data on a carefully prepared copper single-crystal surface.
Table of Contents
- Background to the copper system
- Surface preparation
- Experiment preparation
- Setting the microscope
- Running the microscope
- Moire pattern formation on Cu (111)
- Problems with imaging.
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