NMR of quadrupolar nuclei in solid materials

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書誌事項

NMR of quadrupolar nuclei in solid materials

editors, Roderick E. Wasylishen, Sharon E. Ashbrook, Stephen Wimperis

（EMR handbooks）

Wiley, c2012

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Includes index

内容説明・目次

内容説明

NMR OF QUADRUPOLAR NUCLEI IN SOLID MATERIALS Over the past 20 years technical developments in superconducting magnet technology and instrumentation have increased the potential of NMR spectroscopy so that it is now possible to study a wide range of solid materials. In addition, one can probe the nuclear environments of many other additional atoms that possess the property of spin. In particular, it is possible to carry out NMR experiments on isotopes that have nuclear spin greater that 1/2 (i.e. quadrupolar nuclei). Since more that two-thirds of all NMR active isotopes are quadrupolar nuclei, applications of NMR spectroscopy with quadrupolar nuclei are increasing rapidly. The purpose of this handbook is to provide under a single cover the fundamental principles, techniques and applications of quadrupolar NMR as it pertains to solid materials. Each chapter has been prepared by an expert who has made significant contributions to out understanding and appreciation of the importance of NMR studies of quadrupolar nuclei in solids. The text is divided into three sections: The first provides the reader with the background necessary to appreciate the challenges in acquiring and interpreting NMR spectra of quadrupolar neclei in solids. The second presents cutting-edge techniques and methodology for employing these techniques to investigate quadrupolar nuclei in solids. The final section explores applications of solid-state NMR studies of solids ranging from investigations of dynamics, characterizations of biological samples, organic and inorganic materials, porous materials, glasses, catalysts, semiconductors and high-temperature superconductors. About EMR Handbooks The Encyclopedia of Magnetic Resonance (EMR) publishes a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence-of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of Encyclopedia articles. In consultation with the EMR Editorial Board, the EMR Handbooks are coherently planned in advance by specially-selected Editors, and new articles, are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this handbook and the complete content of the Encyclopedia of Magnetic Resonance at your fingertips! Visit: www.wileyonlinelibrary.com/ref/emr

目次

Contributors ix Series Preface xiii Volume Preface xv Part A: Basic Principles 1 1 Quadrupolar Interactions Pascal P. Man 3 2 Quadrupolar Nuclei in Solids Alexander J. Vega 17 3 Quadrupolar Coupling: An Introduction and Crystallographic Aspects Sharon E. Ashbrook, Stephen Wimperis 45 4 Quadrupolar Nuclei in Solids: Influence of Different Interactions on Spectra David L. Bryce, Roderick E. Wasylishen 63 Part B: Advanced Techniques 75 5 Acquisition of Wideline Solid-State NMR Spectra of Quadrupolar Nuclei Robert W. Schurko 77 6 Sensitivity and Resolution Enhancement of Half-Integer Quadrupolar Nuclei in Solid-State NMR Thomas T. Nakashima, Roderick E. Wasylishen 95 7 Quadrupolar Nutation Spectroscopy Arno P.M. Kentgens 107 8 Dynamic Angle Spinning Philip J. Grandinetti 121 9 Double Rotation (DOR) NMR Ray Dupree 133 10 MQMAS NMR: Experimental Strategies Jean-Paul Amoureux, Marek Pruski 143 11 STMAS NMR: Experimental Advances Sharon E. Ashbrook, Stephen Wimperis 163 12 Correlation Experiments Involving Half-Integer Quadrupolar Nuclei Michael Deschamps, Dominique Massiot 179 13 Computing Electric Field Gradient Tensors Josef W. Zwanziger 199 Part C: Applications 211 14 Quadrupolar NMR to Investigate Dynamics in Solid Materials Luke A. O'Dell, Christopher I. Ratcliffe 213 15 Alkali Metal NMR of Biological Molecules Gang Wu 233 16 Nitrogen-14 NMR Studies of Biological Systems Luminita Duma 255 17 Oxygen-17 NMR Studies of Organic and Biological Molecules Gang Wu 273 18 Oxygen-17 NMR of Inorganic Materials Sharon E. Ashbrook, Mark E. Smith 291 19 Chlorine, Bromine, and Iodine Solid-State NMR David L. Bryce, Cory M. Widdifield, Rebecca P. Chapman, Robert J. Attrell 321 20 Quadrupolar NMR of Ionic Conductors, Batteries, and other Energy-Related Materials Frederic Blanc, Leigh Spencer, Gillian R. Goward 349 21 Quadrupolar NMR of Nanoporous Materials Mohamed Haouas, Charlotte Martineau, Francis Taulelle 371 22 Quadrupolar NMR in the Earth Sciences Jonathan F. Stebbins 387 23 Quadrupolar NMR of Superconductors Nicholas J. Curro 401 24 Quadrupolar NMR of Semiconductors James P. Yesinowski 417 25 Quadrupolar NMR of Metal Nuclides in Biological Materials Tatyana Polenova, Andrew S. Lipton, Paul D. Ellis 439 26 Nuclear Waste Glasses: Insights from Solid-State NMR Scott Kroeker 453 27 Quadrupolar Metal NMR of Oxide Materials Including Catalysts Olga B. Lapina, Victor V. Terskikh 467 28 Quadrupolar NMR of Intermetallic Compounds Frank Haarmann 495 Index 511

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