Material characterization techniques and applications

Author(s)

    • Ortega, Euth Ortiz
    • Hosseinian, Hamed
    • Meza, Ingrid Berenice Aguilar
    • López, María José Rosales
    • Vera, Andrea Rodríguez
    • Hosseini, Samira

Bibliographic Information

Material characterization techniques and applications

Euth Ortiz Ortega ... [et al.]

(Progress in optical science and photonics / series editor, Javid Atai, v. 19)

Springer, c2022

  • : hbk

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Includes bibliographies

Other authors: Hamed Hosseinian, Ingrid Berenice Aguilar Meza, María José Rosales López, Andrea Rodríguez Vera, Samira Hosseini

Description and Table of Contents

Description

This book presents commonly applied characterization techniques in material science, their brief history and origins, mechanism of operation, advantages and disadvantages, their biosensing applications, and troubleshooting for each technique, while addressing the challenges researchers face when working with these techniques. The book dedicates its focus to identifying physicochemical and electrochemical nature of materials including analyses of morphology, mass spectrometry, and topography, as well as the characterization of elemental, structural, thermal, wettability, electrochemical, and chromatography properties. Additionally, the main features and benefits of using coupled characterization techniques are discussed in this book.

Table of Contents

Chapter 1. Morphology Analysis Abstract 1.1 Optical microscopy (OM) 1.1.1 History 1.1.2 Mechanism of operation 1.1.3 Advantages and disadvantages 1.1.4 Applications 1.2 Scanning Electron Microscopy (SEM) 1.2.1 History 1.2.2 Mechanism of operation 1.2.3 Advantages and disadvantages 1.2.4 Applications 1.3 Transmission Electron Microscopy Analysis (TEM) 1.3.1 History 1.3.2 Mechanism of operation 1.3.3 Advantages and disadvantages 1.3.4 Applications Troubleshooting References Chapter 2. Mass Spectrometry Analysis Abstract 2.1 Mass Spectrometry (MS) 2.1.1 History 2.1.2 Mechanism of operation 2.1.3 Advantages and disadvantages 2.1.4 Applications 2.2 Matrix-Assisted Laser Desorption/Ionization - Time-Of-Flight (MALDI-TOF) Spectrometry 2.2.1 History 2.2.2 Mechanism of operation 2.2.3 Advantages and disadvantages 2.2.4 Applications Troubleshooting References Chapter 3. Topography Analysis Abstract 3.1 Atomic Force Microscopy (AFM) 3.1.1 History 3.1.2 Mechanism of operation 3.1.3 Advantages and disadvantages 3.1.4 Applications 3.2 RAMAN Spectroscopy 3.2.1 History 3.2.2 Mechanism of operation 3.2.3 Advantages and disadvantages 3.2.4 Applications Troubleshooting References Chapter 4. Chemical and Structural Analysis Abstract 4.1 RAMAN Spectroscopy 4.1.1 History 4.1.2 Mechanism of operation 4.1.3 Advantages and disadvantages 4.1.4 Applications 4.2 Fourier Transform Infrared Spectroscopy (FTIR) 4.2.1 History 4.2.2 Mechanism of operation 4.2.3 Advantages and disadvantages 4.2.4 Applications 4.3 Ultraviolet-visible Spectroscopy (UV-Vis) 4.3.1 History 4.3.2 Mechanism of operation 4.3.3 Advantages and disadvantages 4.3.4 Applications 4.4 X-ray Photoelectron Spectroscopy (XPS) 4.4.1 History 4.4.2 Mechanism of operation 4.4.3 Advantages and disadvantages 4.4.4 Applications 4.5 Diffuse Reflectance Infrared Fourier Transform Spectroscopy (DRIFTS) 4.5.1 History 4.5.2 Mechanism of operation 4.5.3 Advantages and disadvantages 4.5.4 Applications 4.6 X-Ray Diffraction (XRD) 4.6.1 History 4.6.2 Mechanism of operation 4.6.3 Advantages and disadvantages 4.6.4 Applications 4.7 Nuclear Magnetic Resonance (NMR) 4.7.1 History 4.7.2 Mechanism of operation 4.7.3 Advantages and disadvantages 4.7.4 Applications Troubleshooting References Chapter 5. Thermal Analysis Abstract 5.1 Thermal Gravimetric Analysis (TGA) 5.1.1 History 5.1.2 Mechanism of operation 5.1.3 Advantages and disadvantages 5.1.4 Applications 5.2 Differential scanning calorimetry (DSC) 5.2.1 History 5.2.2 Mechanism of operation 5.2.3 Advantages and disadvantages 5.2.4 Applications 5.3 Differential thermal analysis (DTA) 5.3.1 History 5.3.2 Mechanism of operation 5.3.3 Advantages and disadvantages 5.3.4 Applications Troubleshooting References Chapter 6. Wettability analysis Abstract 6.1 Water Contact Angle (WCA) 6.1.1 History 6.1.2 Mechanism of operation 6.1.3 Advantages and disadvantages 6.1.4 Applications Troubleshooting References Chapter 7. Electrochemical analysis Abstract 7.1 Cyclic Voltammetry (CV) 7.1.1 History 7.1.2 Mechanism of operation 7.1.3 Advantages and disadvantages 7.1.4 Applications 7.2 Electrochemical Impedance Spectroscopy (EIS) 7.2.1 History 7.2.2 Mechanism of operation 7.2.3 Advantages and disadvantages 7.2.4 Applications Troubleshooting References Chapter 8. Chromatography analysis Abstract 8.1 Gas Chromatography (GC) 8.1.1 History 8.1.2 Mechanism of operation 8.1.3 Advantages and disadvantages 8.1.4 Applications 8.2 High-Performance Liquid Chromatography (HPLC) 8.2.1 History 8.2.2 Mechanism of operation 8.2.3 Advantages and disadvantages 8.2.4 Applications 8.3 Ion Chromatography 8.3.1 History 8.3.2 Mechanism of operation 8.3.3 Advantages and disadvantages 8.3.4 Applications 8.4 High Temperature Gel Permeation Chromatography (HT-GPC) 8.4.1 History 8.4.2 Mechanism of operation 8.4.3 Advantages and disadvantages 8.4.4 Applications Troubleshooting References Chapter 9. Coupled Techniques Abstract 9.1 RAMAN-AFM 9.1.1 History 9.1.2 Mechanism of operation 9.1.3 Advantages and disadvantages 9.1.4 Applications 9.2 GC-MS 9.2.1 History 9.2.2 Mechanism of operation 9.2.3 Advantages and disadvantages 9.2.4 Applications 9.3 GPC-MS 9.3.1 History 9.3.2 Mechanism of operation 9.3.3 Advantages and disadvantages 9.3.4 Applications 9.4 SEM-EDX 9.4.1 History 9.4.2 Mechanism of operation 9.4.3 Advantages and disadvantages 9.4.4 Applications 9.5 UV-Vis-CV 9.5.1 History 9.5.2 Mechanism of operation 9.5.3 Advantages and disadvantages 9.5.4 Applications Troubleshooting References Table of abbreviations

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