Handbook for chemical process research and development
著者
書誌事項
Handbook for chemical process research and development
CRC Press, 2023
2nd ed
- : hbk
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注記
Includes index
内容説明・目次
内容説明
This unique volume now in its second edition is designed to provide readers with an unprecedented strategy and approach which will help chemists and graduate students develop chemical processes in an efficient manner
Promotes an industrial mindset concerning safety and commercial viability when developing methods
The author discusses development strategies with case studies and experimental procedures
Focuses on mechanism-guided process development which provides readers with practical strategies and approaches
Addresses more common process issues such as safety, cost, robustness, and environmental impact.
目次
1. Reaction solvent selection
2. Reagent selection
3. Various reagent surrogates
4. Modes of reagent addition -control of impurity formation
5. Process optimization with additives
6. Process optimization of catalytic reactions
7. Process optimization of problematic reactions
8. Hazards of oxidation and reduction reactions
9. Other hazardous reactions
10. Hazardous reagents
11. Grignard reagent and related reactions
12. Challenging reaction intermediates
13. Protecting groups
14. Telescope approach
15. Design of new synthetic route
16. Stereochemistry
17. Various quenching strategies
18. Various isolation and purification strategies
19. Methods for residual metal removal
20. Methods for impurity removal
21. Pharmaceutical salts
22. Solid form
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