Basic gas chromatography

著者

• McNair, Harold Monroe
• Miller, James M.
• Snow, Nicholas H.

書誌事項

Basic gas chromatography

Harold M. McNair, James M. Miller, Nicholas H. Snow

John Wiley & Sons, 2019

3rd ed

タイトル別名

Gas chromatography

注記

Includes bibliographical references (p. 238-239) and index

内容説明・目次

内容説明

Basic Gas Chromatography, Third Edition provides a brief introduction to GC following the objectives for titles in this series. It should appeal to readers with varying levels of education and emphasizes a practical, applied approach to the subject. : This book provides a quick need-to-know introduction to gas chromatography; still the most widely used instrumental analysis technique, and is intended to assist new users in gaining understanding quickly and as a quick reference for experienced users. The new edition provides updated chapters that reflect changes in technology and methodology, especially sample preparation, detectors and multidimensional chromatography. The book also covers new detectors recently introduced and sample preparation methods that have become much more easily accessible since the previous edition.

目次

Preface to the Third Edition xi Preface to the Second Edition xiii Preface to the First Edition xv Acknowledgments xvii 1 Introduction 1 A Brief History 1 Definitions 3 Overview: Advantages and Disadvantages 9 Instrumentation and Columns 12 References 14 2 Basic Concepts and Terms 15 Definitions, Terms, and Symbols 15 The Rate Theory 25 The Achievement of Separation 34 References 35 3 Instrument Overview 37 Carrier Gas 38 Flow Control and Measurement 39 Sample Inlets and Sampling Devices 42 Capillary Columns 46 Temperature Zones 47 Detectors 49 Data Systems 50 Reference 50 4 Capillary Columns 51 Types of Capillary Columns 51 Capillary Column Tubing 54 Advantages of Capillary Columns 55 Column Selection 57 Column Quality Testing: The Grob Test Mix 65 Special Troubleshooting Considerations for Capillary Columns 66 Guidelines for Selecting Capillary Columns 67 References 68 5 Stationary Phases 69 Selecting a Column 69 Common and Important Stationary Phases 81 Other Common Stationary Phases 83 References 86 6 Temperature Programming 87 Advantages and Disadvantages of TPGC 89 Requirements for TPGC 90 Example Temperature Programmed Chromatograms 91 Special Topics 96 References 98 7 Inlets 99 Inlet Fundamentals 99 Split Inlet 101 Splitless Inlet 104 On-Column Inlet 106 Programmed Temperature Vaporizer (PTV) 107 Related Topics 108 References 111 8 Classical Detectors: FID, TCD, and ECD 113 Classification of Detectors 115 Common Detector Characteristics 117 Flame Ionization Detector (FID) 124 Thermal Conductivity Detector (TCD) 128 Electron Capture Detector (ECD) 131 Other Detectors 134 References 136 9 Qualitative and Quantitative Analysis 139 Qualitative Analysis 139 Quantitative Analysis 145 Statistics of Quantitative Calculations 145 Quantitative Analysis Methods 148 Summary 154 References 154 10 GC-MS and Spectrometric Detectors 157 Gas Chromatography-Mass Spectrometry (GC-MS) 158 Gas Chromatography-Mass Spectrometry-Mass Spectrometry (GC-MS-MS) 171 Gas Chromatography-Fourier Transform Infrared Spectrometry (GC-FITR) 172 Gas Chromatography-Vacuum Ultraviolet (GC-VUV) Spectrometry 172 References 174 11 Sampling Methods 177 Overview 177 Liquid-Liquid Extraction (LLE) 179 Solid-Liquid Extraction: Soxhlet Extraction and Accelerated Solvent Extraction (ASE) 182 Solid-Phase Extraction 183 Liquid-Vapor or Solid-Vapor Extraction: Headspace Extraction 186 Solid-phase microextraction (SPME) 188 QuEChERS (Quick, Easy Cheap, Effective, Rugged, Safe) 192 Additional Techniques and Summary 193 References 194 12 Multidimensional Gas Chromatography 197 Overview 197 Fundamental Principles of Multidimensional Chromatography 198 Heart Cutting 202 Comprehensive Two-Dimensional GC (GCxGC) 203 LC-GC with Heart Cutting 206 Comprehensive LCxGC 206 References 208 13 Packed Column GC 211 Columns 211 Solid Supports and Stationary Phases 213 Liquid Stationary Phases 214 Solid Stationary Phases 215 Gas Analysis 218 Analysis of Other Inorganics 221 Inlets and Liquid Sampling for Packed Columns 221 Special Columns and Applications 222 References 224 14 Special Topics 225 Fast GC 225 Chiral Analysis by GC 228 Analysis of Nonvolatile Compounds 229 Pyrolysis 233 Inverse GC 233 Additional Theory 234 Activity Coefficients 236 References 238 15 Troubleshooting GC Systems 241 Preventing Problems 241 Troubleshooting Problems 243 Appendix A Acronyms, Symbols and Greek Symbols 251 Appendix B Some Internet Sites for Gas Chromatography 255 Appendix C Other Books On Gas Chromatography 257 Index 259

「Nielsen BookData」 より

詳細情報

• NII書誌ID(NCID): BD05647809
• ISBN:
  • 9781119450757
• 出版国コード: us
• タイトル言語コード: eng
• 本文言語コード: eng
• 出版地: Hoboken, N.J.
• ページ数/冊数: xvii, 265 p.
• 大きさ: 24 cm
• 分類:
  • LCC : QD79.C45
  • DC23 : 543/.85
• 件名:
  • LCSH : Gas chromatography