Laboratory techniques in organic chemistry : supporting inquiry-driven experiments
著者
書誌事項
Laboratory techniques in organic chemistry : supporting inquiry-driven experiments
W.H. Freeman, c2014
4th ed. / Jerry R. Mohrig [et al.]
- pbk
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注記
Other author: David G. Alberg, Gretchen E. Holifmeister, Paul F. Schatz, Christina Noring Hammond
Includes bibliographical references and index
内容説明・目次
内容説明
The most comprehensive textbook and detailed presentation of the lab techniques organic chemistry students need to know. Compatible with any organic chemistry lab manual or set of experiments, it combines specific instructions for three different kinds of laboratory glassware: miniscale, standard taper microscale, and Williamson microscale. This title provides effective support to all those looking for guided-inquiry and design-based experiments and projects, as well as for traditional lab experiments.
This title is for organic students of all levels looking to improve and understand their knowledge of lab work. With new authors David Alberg and Gretchen Hofmeister on board for this fourth edition, both bring copious amounts of experience in organic chemistry. They have been able to revive the writing in the book, while also adding new examples and pitfalls for students to avoid.
目次
PART 1 Introduction to the Organic Laboratory ESSAY The Role of the Laboratory 1. Safety in the Laboratory.- 2. Green Chemistry.- 3. Laboratory Notebooks and Prelaboratory Information.- PART 2 Carrying Out Chemical Reactions ESSAY Learning to Do Organic Chemistry 4. Laboratory Glassware .- 5. Measurements and Transferring Reagents .- 6. Heating and Cooling Methods .- 7. Setting Up Organic Reactions .- 8. Computational Chemistry.- PART 3 Basic Methods for Separation, Purification, and Analysis ESSAY Intermolecular Forces in Organic Chemistry 9. Filtration.- 10. Extraction .- 11. Drying Organic Liquids and Recovering Reaction Products.- 12. Boiling Points and Distillation.- 13. Refractometry.- 14. Melting Points and Melting Ranges.- 15. Recrystallization.- 16. Sublimation.- 17. Optical Activity and Enantiomeric Analysis.- PART 4 Chromatography ESSAY Modern Chromatographic Separations 18. Thin-Layer Chromatography.- 19. Liquid Chromatography.- 20. Gas Chromatography.- PART 5 Spectrometric Characterization Methods ESSAY The Spectrometric Revolution 21. Infrared Spectroscopy.- 22. Nuclear Magnetic Resonance Spectroscopy.- 23. 13C and Two-Dimensional NMR Spectroscopy.- 24. Mass Spectrometry.- 25. Ultraviolet and Visible Spectroscopy.- 26 . Integrated Spectrometry Problems.- PART 6 Designing and Carrying out Organic Experiments.- Essay Inquiry-Driven Lab Experiments 27. Designing Chemical Reactions.- 28. Using the Literature of Organic Chemistry.
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