書誌事項
- タイトル別名
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- Analytical method of triethylamine and tributyliamine in polycarbonate products
- ポリカーボネート セイヒン チュウ ノ トリエチルアミン オヨビ トリブチルアミン ブンセキホウ
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A method for the determination of triethylamine and tributhlamine in polycarbonate products was developed using liquid chromatography coupled with tandem mass spectrometry (LC-MS/MS). The sample was dissolved with dichloromethane, and the polymer was precipitated by addition of methanol. In order to avoid volatilization of triethylamine and tributylamine during evaporation of dichloromethane and methanol, 2% formic acid was added to the methanol mixture. After evaporation, triethylamine and tributylamine were determined by LC-MS/MS. Recoveries of triethylamine and tributylamine in polycarbonate products at the level of 1μg/g were 96,101% respectively, and the limits of quantification were 0.05μg/g in samples.
収録刊行物
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- 日本食品化学学会誌
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日本食品化学学会誌 20 (2), 114-118, 2013
日本食品化学学会
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詳細情報 詳細情報について
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- CRID
- 1390282680172169856
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- NII論文ID
- 110009649308
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- NII書誌ID
- AA11666400
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- ISSN
- 21896445
- 13412094
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- NDL書誌ID
- 024876082
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- 本文言語コード
- ja
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- データソース種別
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- JaLC
- NDL
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可