Microwave-promoted Synthesis of Methoxylated Benzaldehydes from Natural <i>cis</i>-Phenylpropenes Using NaIO4/OsO4 (cat.)

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  • Arun K Sinha
    Natural Plant Products Division, Institute of Himalayan Bioresource TechnologyPalampur (H.P.)-176061 , India
  • Bhupendra P Joshi
    Natural Plant Products Division, Institute of Himalayan Bioresource TechnologyPalampur (H.P.)-176061 , India
  • Ruchi Acharya
    Natural Plant Products Division, Institute of Himalayan Bioresource TechnologyPalampur (H.P.)-176061 , India

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Abstract

<jats:title>Abstract</jats:title> <jats:p>Microwave-promoted rapid oxidation of toxic natural cis-phenylpropenes (1a–1e) into high valued methoxylated benzaldehydes (2a–2e) was achieved within 2 min in high yield (71–84%) by reacting with sodium metaperiodate in the presence of catalytic amount of osmium tetraoxide (co-oxidant) and benzyltriethylammonium chloride (PTC).</jats:p>

Journal

  • Chemistry Letters

    Chemistry Letters 32 (8), 780-781, 2003-07-30

    Oxford University Press (OUP)

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