Organic syntheses : an annual publication of satisfactory methods for the preparation of organic chemicals

著者

• Kende, Andrew S.
• Heathcock, Clayton H.
• Coates, Robert M. (Robert Myron)
• Martin F. Semmelhack
• Smart, Bruce E.
• Paquette, Leo A.

書誌事項

Organic syntheses : an annual publication of satisfactory methods for the preparation of organic chemicals

board of editors, Andrew S. Kende ... [et al.]

Wiley, 1961-1990

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• v. 42
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• v. 58(1978)
• v. 59(1979)
• v. 60(1981)
• v. 61(1983)
• v. 62
• v. 63
• v. 64
• v. 65(1987)
• v. 66(1988)
• v. 67(1989)
• v. 68(1990)
• v. 69(1990)
• v. 70(1992)

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すべて表示

注記

Vol. 59: Robert M. Coates, editor in chief

Vol. 60: Orville L. Chapman, editor in chief

Vol. 61: Robert V. Stevens, editor in chief

Vol. 62: Martin F. Semmelhack, editor in chief

Vol. 63: Gabriel Saucy, editor in chief

Vol. 65: Edwin Vedejs, editor-in-chief

Vol. 66: Heathcock, Clayton H., editor-in-chief

Vol. 67: Bruce E. Smart, editor-in-chief

Vol. 68: James D. White, editor-in chief

Vol. 69: Leo A. Paquette, editor-in-chief

Vol. 70: Albert I. Meyers, editor-in-chief

Includes bibliographies and index

Vol. 71以降は別書誌 <BA21024124>

内容説明・目次

巻冊次

v. 67(1989) ISBN 9780471513797

内容説明

Offers 30 reliable, proven preparations--some which demonstrate new general synthetic applications and others for specific compounds of broad interest--focusing on the use of organometallic reagents and synthesis of chiral molecules.

目次

Partial table of contents: Enantiometric (S)-(-)- and (R)-(-)-1,1'-Binaphthyl-2,2'-DiylHydrogen Phosphate (J. Jacques & C. Fouquey). (R)-(-)- and (S)-(-)-2,2'-BIS (Diphenylphosphino)-1,1'-Binaphythyl(Binap) (H. Takaya, et al.). Addition of Dialkylamines to N/Myrcene: N,N-Diethylgeranylamine (K.Takabe, et al.). (-)-Salsolidine (A. Meyers, et al.). Palladium-Catalyzed Coupling of Acid Chlorides with OrganotinReagents: Ethyl (E)-4-(4-Nitro-Phenyl)-4-OXO-2-Butenoate (A.Renaldo, et al.). 4,4-Dimethyl-2-Cyclopenten-1-One (D. Pauley, et al.). Ethynyl p-Tolyl Sulfone (L. Waykole & L. Paquette). Methyl 7-Hydroxyhept-5-Ynoate (G. Casy, et al.). 4-Methoxy-3-Penten-2-One (G. Kraus, et al.).

巻冊次

v. 68(1990) ISBN 9780471537892

内容説明

An update to the continuing series containing 31 edited and checked preparations that represent the most active and advanced areas in organic synthesis. These procedures are presented in six categories: simple one- and two- carbon synthons, chiral auxiliaries and stereocontrolled processes, organometallic reagents, useful starting materials for complex syntheses, new reactions of potentially broad utility and cryptands with novel guest-host properties.

目次

Partial table of contents: Trimethylsilyldiazomethane (T. Shioiri, et al.). Acetyltrimethylsilane (J. Soderquist). 3-Butylcyclobutenone (R. Danheiser, et al.). Allyltributyltin (N. Halligan & L. Blaszczak). Allylic Acetoxylation of Cycloalkenes: 2-Cyclohepten-1-Yl Acetate(A. Heumann, et al.). 3-Methyl-2(5H)-Furanone (J. Nasman). The Carroll Rearrangement: 5-Dodecen-2-One (S. Wilson & C.Augelli). Cumulative Author Index for Volumes 65-68. Cumulative Subject Index for Volumes 65-68.

巻冊次

v. 69(1990) ISBN 9780471545606

内容説明

Like its predecessors, this volume contains checked and edited procedures for dealing with important new synthetic methods or specific compounds holding potential interest for synthetic chemists. Among the organic procedures covered are: kinetic resolution by enzymatic means, stereocontrolled processes that have proven useful for constructing relative complex molecules, the vital role that organometallic reagents play in the transformation of functional groups, preparations of starting materials that play an established role in important structural transformation and/or multistep syntheses, the preparation of oxaziridine--a selective, aprotic oxidizing agent of considerable importance, and a chiral auxiliary that has found substantial use in asymmetric reactions of various types.

目次

Partial table of contents: Enantiomerically Pure Ethyl (R)- and (S)-2-Fluoro-Hexanoate byEnzyme-Catalyzed Kinetic Resolution (P. Kalaritis & R.Regenye). 1,3,4,6-Tetra-O-Acetyl-2-Deoxy--D-Glucopyranose (B. Giese & K.Groninger). Mixed Higher Order Cyanocuprate-Induced Epoxide Openings:1-Benzyloxy-4-Penten-2-OL (B. Lipshutz, et al.). Hydromagnesiation Reaction of Propargylic Alcohols:(E)-3-Pentyl-2-Nonene-1, 4-Diol from 2-Octyn-1-OL (F. Sato & Y.Kobayashi). N-Fluoropyridinium Triflate: An Electrophilic Fluorinating Agent(T. Umemoto, et al.). Methyl 2-Chloro-2-Cyclo-Propylidenacetate (T. Liese, et al.). Unchecked Procedures. Cumulative Author Index for Volumes 65, 66, 67, 68, and 69. Cumulative Subject Index for Volumes 65, 66, 67, 68, and 69.

巻冊次

v. 70(1992) ISBN 9780471577430

内容説明

In keeping with the tradition of this highly successful and respected series, Volume 70 contains 31 procedures, carefully checked and edited by independent laboratories. For the first time, procedures are accompanied by a new section on waste disposal data. This includes any special disposal of chemical waste utilized by the submitters in order to comply with modern, clean disposal practices of toxic materials. This monograph should be consulted by all users of these volumes, in keeping with current trends to preserve the environment.

目次

Partial table of contents: Synthesis of N-tert-Butoxy-Carbonyl-L-Serine beta-Lactone and thep-Toluenesulfonic Acid Salt of (S)-3-Amino-2-Oxetanone (S. Pansare,et al.). 1,1,-Dimethylethyl (S)-Or(R)-4-Formyl-2,2-Dimethyl-3-Oxazolidinecarboxylate: A UsefulSerinal Derivative (P. Garner & J. Park). N-(Benzyloxycarbonyl)-L-Vinylglycine Methyl Ester (M. Carrasco, etal.). (R)-(-)-10-Methyl-1(9)-Octal-2-One (G. Revial & M. Pfau). (R,R)-1,2-Diphenyl-1,2-Ethanediol (Stilbene Diol) (B. McKee, etal.). A Stable Chiral 1,4-Dihydro-Pyridine Equivalent for the AsymmetricSynthesis of Substituted Piperidines:2-Cyano-6-Phenyloxazolo-Piperidine (M. Bonin, et al.). (S)-(-)-and (R)-(+)-1,1'-Bi-2-Naphthol (R. Kazlauskas). 9-Thiabicyclo{3.3.1} Nonane-2,6-Dione (R. Bishop). Tris(Trimethylsilyl)Silane (J. Dickhaut & B. Giese). Spiroannelation Via Organobis-(Cuprates):9,9-Dimethylspiro-{4.5}Decan-7-One (P. Wender, et al.). 1-Phenyl-2,3,4,5-Tetramethyl-Phosphole (P. Fagan & W.Nugent). Unchecked Procedures. Indexes.

巻冊次

v. 66(1988) ISBN 9780471619727

内容説明

The latest volume in this annual series maintains the purpose of earlier volumes: to provide reliable procedures for the preparation of specific compounds, and to demonstrate general procedures of wider application. When demonstrating a procedure, the editors have chosen to select an application for which that procedure is superior to other available methods for the specific product. Volume 66 contains 28 preparations that illustrate many of the most active areas in synthetic organic chemistry.

巻冊次

v. 65(1987) ISBN 9780471636373

内容説明

This volume reflects the intensive activity in several areas of synthetic organic chemistry, such as enol/carbonyl condensations; alkynes, alkenes and aromatic carbocycles; heteroelement chemistry (with respect to organosilicon reagents, transition element chemistry, and in the preparation of-lactams and indoles); and chiral auxiliaries.

目次

Partial table of contents: Acetone Trimethylsilyl Enol Ether (N. Walshe et al.). 3-Hydroxy-3-Methyl-1-Phenyl-1-Butanone by Crossed Aldol Reaction(T. Mukaiyama, K. Narasaka). Ring Expansion and Cleavage of Succinoin Derivatives:Spiro[4.5]Decane-1, 4-Dione and Ethyl 4-Cyclohexyl-4-Oxobutanoate(E. Nakamura, I. Kuwajima). Preparation and Three-Carbon / Two Carbon Cycloaddition of a Cyclopropenone Ketal: Cyclo-Propenone1,3-Propanediol Ketal (D. Boger et al.). 1,2,3,4,5-Pentamethylcyclo-Pentadiene (R. Threlkel et al.). Methylenation of Carbonyl Compounds: (/)-3-Methylene-cis-p-Methane(L. Lombardo). A General Synthetic Method for the Preparation of Conjugated Dienesfrom Olefins Using Bromomethanesulfonyl Bromide:1,2-Dimethylenecyclohexane (E. Block, M. Aslamb). Unchecked Procedures. Cumulative Author Indexes for Volume 65. Cumulative Subject Indexes for Volume 65.

巻冊次

v. 63 ISBN 9780471829409

内容説明

This annual volume in the series contains 28 checked and edited procedures on stereochemical selection. Eight procedures illustrate the impressive advances in the areas of enantioselective (asymmetric) synthesis, four cover, highly stereospecific syntheses of useful optically active products. Procedures are given for two specific compounds - cyclopropanone ethyl hemiketal and hexafluoroacetone, and the rest treat a wide range of synthetic methodology.

目次

• Yeast Reduction of Ethyl Acetoacetate: (S)-(+)-Ethyl 3-Hydroxybutanoate
• Preparation of Chiral, Non- Racemic +gg-Lactones by Enzyme-Catalyzed Oxidation of Meso-Diols: (+)-(1R, 6S)-8-Oxabicyclo 4.3.0 Nonan-7-One
• Asymmetric Hydrogenation of Ketopantoyl Lactones: D-(-)-Patnoyl Lactone
• (+)-(7aS)-2, 3, 7, 7a-Tetrahydro-7-a-Methyl-1 H-Idene-1, 5-(6H)- Dione
• Asymmetric Synthesis of S-8a-Methyl-3, 4, 8, 8a-Tetra- hydro-1, 6 (2H, 7H)-Naphthalenedione
• Asymmetric Hydroboration of 5-Substituted Cyclopentadienes: Synthesis of Methyl (1R, 5R)-5 Hydroxy-2-Cyclopentene-1-Acetate
• Asymmetric Reduction of +ga, +gb-Acetylenic Ketones with B-3-Pinanyl-9-Borabicyclo- 3.3.1 Nonane: (R)-(+)-1-Octyn-3-OL
• Enantioselective Epoxidation of Allylic Alcohols: (2S, 3S)-3-Propyloxiranemethanol
• 2-Methyl-2- Trimethylsilyloxtpentan-3-One
• (2SR, 3RS)-2, 4-Dimethyl-3- Hydroxypentanoic Acid
• (2SR, 3RS)-2, 4-Dimethyl-3- Hydrocypentanoic Acid
• Diastereoselective +ga-Alkylation of +gb- Hydroxycarboxylic Esters Through Alkoxide Enolates: (+)-Diethyl (2S, 3R)-3-Allyl-2-Hydroxysucciante from (-)-Diethyl S-Malate

巻冊次

v. 64 ISBN 9780471847427

内容説明

The current volume continues the tradition of providing significant and interesting procedures, which should prove worthwhile to many synthetic chemists working in increasingly diverse areas. Following precedent, there is no specific or central theme to this volume.

目次

Partial table of contents: Addition of An Ethylcopper Complex to 1-Octyne: (E)-5-Ethyl-1,4-Undecadiene. 2-Alkenyl Carbinols From 2-Halo Ketones. -Amino Acetals. Cyclobutene. Deoxygenation of Secondary Alcohols. DI-tert-BUTYL Methylenemalonate. The Stork-Danheiser Kinetic Alkylation Procedure. Diethyl Phosphonate. 1,3-Dimethylimidazole - 2 Thione. Ethyl Isocrotonate. Formyl Transfer to Grignard Reagents. -Hydroxylation of a Keytone Using o-Iodosylbenzoic Acid. Phenyl Vinyl Sulfone and Sulfoxide. Stereospecific Reduction of Propargyl Alcohols. Trifluoroacetyl Triflate. Cumulative Author Index for Vols. 60-64. Cumulative Subject Index for Vols. 60-64.

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詳細情報

• NII書誌ID(NCID): BA00241860
• ISBN:
  • 0471972401
  • 0471942103
  • 0471103047
  • 0471067857
  • 047141560X
  • 0471106151
  • 0471428361
  • 0471573906
  • 0471022187
  • 0471032352
  • 0471047392
  • 0471059633
  • 0471093599
  • 0471870382
  • 0471817864
  • 0471829404
  • 0471847429
  • 0471636371
  • 0471619728
  • 0471513792
  • 0471537896
  • 0471545600
  • 047157743X
• LCCN: 21017747
• 出版国コード: us
• タイトル言語コード: eng
• 本文言語コード: eng
• 出版地: New York
• ページ数/冊数: 30 v.
• 大きさ: 24 cm
• 分類:
  • LCC : QD1
  • LCC : QD262
  • DC : 540/.8 s
  • DC19 : 547/.2
  • NDC8 : 434
  • NDC7 : 434.9
• 件名:
  • LCSH : Chemistry, Organic -- Synthesis -- Addresses, essays, lectures