Organic syntheses
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Bibliographic Information
Organic syntheses
John Wiley & Sons, 1932-
A rev. ed. of annual volumes
- collective v. 1
- collective v. 2
- collective v. 3
- collective v. 4
- collective v. 5
- collective v. 6
- collective v. 7
- collective v. 8
- collective v. 9
- collective v. 10
- collective v. 11
- collective v. 12
Access to Electronic Resource 7 items
Available at / 147 libraries
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Osaka Kyoiku University Library
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Okayama University Library, Shikata Branch Library鹿田図
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Kanazawa University Library自然図自動書庫
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Science and Technology Library, Kyushu University
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Kyoto Institute of Technology Library図
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Katsura Library, Kyoto University図
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Kyoto Pharmaceutical University Library
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Kindai University Central Library中図
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National Institute of Technology, Gunma College Library図書
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Kochi University of Technology.Library
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Kobe Shoin Women's University Library / Kobe Shoin Women's College Library
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Kobe University Library for Maritime Sciences
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National Institutes of Natural Sciences Okazaki Library and Information Center図
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Engineering Library, Shinshu University
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Faculty of Textile Science and Technology Library, Shinshu University研究室
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Agricultural Library, Shinshu Univ.
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The University of Electro-Communications Library参考
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The University of Electro-Communications Library図庫
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Etchujima library, Tokyo University of Marine Science and Technology図
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Tokyo Metropolitan University Library
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Tokyo University of Agriculture and Technology Koganei Library
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University of Toyama Library, Central Library工室
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Toyohashi University of Technology Library図
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Nagoya University Library農高分生材
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Digital Library of Nara Institute of Science and Technology
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Himeji Dokkyo University Library図
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University of Teacher Education Fukuoka Library図
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Note
Vol. 1: Being a revised edition of annual volumes I-IX; Henry Gilman, editor-in-chief
Vol. 2: A revised edition of Annual volumes X-XIX; A.H. Blatt, editor-in-chief
Vol. 3: A revised edition of Annual volumes 20-29; E.C. Horning, editor-in-chief
Vol. 4: A revised edition of Annual volumes 30-39; Norman Rabjohn, editor-in-chief
Vol. 5: A revised edition of Annual volumes 40-49; Henry E. Baumgarten, editor-in-chief
Vol. 6: A revised edition of Annual volumes 50-59; Wayland E. Noland, editor-in-chief
Vol. 7: A revised edition of Annual volumes 60-64; Jeremiah P.Freeman, editor-in-chief
Vol. 8: A revised edition of Annual volumes 65-69; Jeremiah P. Freeman, editor-in-chief
Vol. 9: A revised edition of Annual volumes 70-74; Jeremiah P. Freeman, editor-in-chief
Vol. 10: A revised edition of Annual volumes 75-79; Jeremiah P. Freeman, editor-in-chief
Vol. 11: A revised edition of Annual volumes 80-84
Vol. 12: A revised edition of Annual volumes 85-89; Rick L. Danheiser, editor-in-chief
The place of publication of Vol.11: Hoboken, New Jersey
The place of publication of Vol.12: Hoboken, New Jersey
Description and Table of Contents
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collective v. 11 ISBN 9780470395486
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collective v. 5 ISBN 9780471057079
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collective v. 2 ISBN 9780471079866
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collective v. 9 ISBN 9780471242482
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Table of Contents
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collective v. 3 ISBN 9780471409533
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collective v. 10 ISBN 9780471445296
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Table of Contents
- 7 -ACETOXY-(1H , 6H )-BICYCLO[4.4.1]UNDECA-2,4,8-TRIENE VIA CHROMIUMMEDIATED HIGHER ORDER CYCLOADDITION. STILLE COUPLINGS CATALYZED BY PALLADIUM-ON-CARBON WITH CUI AS A COCATALYST: SYNTHESIS OF 2-(4'-ACETYLPHENYL)THIOPHENE. ASYMMETRIC SYNTHESIS OF -AMINO ACIDS BY THE ALKYLATION OF PSEUDOEPHEDRINE GLYCINAMIDE: L-ALLYLGLYCINE AND N-Boc-L-ALLYLGLYCINE. 2-AMINO-3-FLUOROBENZOIC ACID. (1S,2R)-1-AMINOINDAN-2-OL. SYNTHESIS OF cis-4a(S),8a(R)-PERHYDRO-6(2H)-ISOQUINOLINONES FROM QUININE: 4a(S), 8a(R)-2-BENZOYLOCTAHYDRO-6(2H)-ISOQUINOLINONE. N-BENZYL-2,3-AZETIDINEDIONE. SULFINIMINES (THIOOXIMINE S-OXIDES): ASYMMETRIC SYNTHESIS OF METHYL (R)-(th)-b-PHENYLALANATE FROM (S)-(th)-N-(BENZYLIDENE)-p-TOLUENESULFINAMIDE. 2-(N-BENZYL-N-MESITYLENESULFONYL)AMINO-1-PHENYL-1-PROPYL PROPIONATE. REGIOSELECTIVE MONOALKYLATION OF KETONES VIA THEIR MANGANESE ENOLATES: 2-BENZYL-6-METHYLCYCLOHEXANONE FROM 2-METHYLCYCLOHEXANONE. SYNTHESIS OF (-)-(E.S)-3-(BENZYLOXY)-1-BUTENYL PHENYL SULFONE VIA A HORNER-WADSWORTH- EMMONS REACTION OF (-)-(S)-2-(BENZYL OXY)PROPANAL. 1-[N-BENZYLOXYCARBONYL-(1S)-1-AMINO-2-OXOETHYL]-4-METHYL-2,6,7-TRIOXABICYCLO[2.2.2]OCTANE. (3,4,5-TRIFLUOROPHENYL)BORONIC ACID-CATALYZED AMIDE FORMATION FROM CARBOXYLIC ACIDS AND AMINES: N-BENZYL-4-PHENYLBUTYRAMIDE. PHOTOCHEMICAL SYNTHESIS OF BICYCLO[1.1.1]PENTANE-1,3-DICARBOXYLIC ACID. BICYCLOPROPYLIDENE. RESOLUTION OF 1,1'-Bi-2-NAPHTHOL. (R,R)-N,N'-BIS(3,5-DI-tert-BUTYLSALICYLIDENE-1,2-CYCLOHEXANEDIAMINO MANGANESE(III) CHLORIDE, A HIGHLY ENANTIOSELECTIVE EPOXIDATION CATALYST. SYNTHESIS OF UNSYMMETRICAL BIARYLS USING A MODIFIED SUZUKI CROSSCOUPLING: 4-BIPHENYLCARBOXALDEHYDE. EFFICIENT SYNTHESIS OF HALOMETHYL-2,2'-BIPYRIDINES: 4,4'-BIS(CHLOROMETHYL)-2,2'-BIPYRIDINE. (R)-(+)- AND (S)-(-)-2,2'-BIS-(DIPHENYLPHOSPHINO)-1,1'-BINAPHTHYL (BINAP). BIS(PINACOLATO)DIBORON. PREPARATION OF BIS(2,4,6-TRIMETHYLPYRIDINE)IODINE(I) HEXAFLUOROPHOSPHATE AND BIS(2,4,6-TRIMETHYLPYRIDINE)BROMINE(I) HEXAFLUOROPHOSPHATE. 3-(4-BROMOBENZOYL)PROPANOIC ACID. BROMOFLUORINATION OF ALKENES: 1-BROMO-2-FLUORO-2-PHENYLPROPANE. SYNTHESIS OF 4-(2-BROMO-2-PROPENYL)-4-METHYL- -BUTYROLACTONE BY THE REACTION OF ETHYL LEVULINATE WITH (2-BROMOALLYL) DIISOPROPOXYBORANE PREPARED BY HALOBORATION OF ALLENE. DIASTEREOSELECTIVE SYNTHESIS OF PROTECTED VICINAL AMINO ALCOHOLS: (S)-2-[(4S)-N-tert-BUTOXYCARBONYL-2,2-DIMETHYL-1,3-OXAZOLIDINYL]-2-tert-BUTYLDIMETHYLSILOXYETHANAL FROM A SERINE-DERIVED ALDEHYDE. BUTYL 4-CHLOROPHENYL SULFIDE. PHOTOINDUCED-ADDITION OF METHANOL TO (5S)-(5-O-tert-BUTYLDIMETHYLSILOXYMETHYL) FURAN-2(5H)-ONE: (4R,5S)-4-HYDROXYMETHYL-(5-O-tert-BUTYLDIMETHYLSILOXYMETHYL)FURAN-2(5H)-ONE. [3 + 4] ANNULATION USING A [ -(TRIMETHYLSILYL)ACRYLOYL]SILANE AND THE LITHIUM ENOLATE OF AN ?, ?-UNSATURATED METHYL KETONE: (1R*,6S*,7S*)-4-(tert-BUTYLDIMETHYLSILOXY)-6-(TRIMETHYLSILYL)BICYCLO[5.4.0]UNDEC-4-EN-2-ONE. (tert-BUTYLDIMETHYLSILYL)ALLENE. SYNTHESIS AND UTILIZATION OF INDIUM (I) IODIDE FOR IN SITU FORMATION OF ENANTIOENRICHED ALLENYLINDIUM REAGENTS AND THEIR ADDITION TO ALDEHYDES: (2R,3S,4S)-1-(tert-BUTYLDIPHENYLSILYLOXY)-2,4-DIMETHYL-5-HEXYN-3-OL. DIMETHYL SQUARATE AND ITS CONVERSION TO 3-ETHENYL-4-METHOXYCYCLOBUTENE-1,2-DIONE AND 2-BUTYL-6-ETHENYL-5-METHOXY-1,4-BENZOQUINONE. PREPARATION OF 1-BUTYL-3-METHYL IMIDAZOLIUM-BASED ROOM TEMPERATURE IONIC LIQUIDS. PREPARATION AND DIELS-ALDER REACTION OF A 2-AMIDO SUBSTITUTED FURAN: tert-BUTYL 3a-METHYL-5-OXO-2,3,3a,4,5,6-HEXAHYDROINDOLE-1-CARBOXYLATE. (S)-3-(tert-BUTYLOXYCARBONYLAMINO)-4-PHENYLBUTANOIC ACID. USE OF CERIUM(III) CHLORIDE IN THE REACTIONS OF CARBONYL COMPOUNDS WITH ORGANOLITHIUMS OR GRIGNARD REAGENTS FOR THE SUPPRESSION OF ABNORMAL REACTIONS: 1-BUTYL-1,2,3,4-TETRAHYDRO-1-NAPHTHOL. CAMPHORQUINONE AND CAMPHORQUINONE MONOXIME. PHOTO-INDUCED RING EXPANSION OF 1-TRIISOPROPYLSILYLOXY-1-AZIDOCYCLOHEXANE: PREPARATION OF e-CAPROLACTAM. 3-CHLORO-2-(CHLOROMETHYL)-1-PROPENE. 1-CHLORO-(2S,3S)-DIHYDROXYCYCLOHEXA-4,6-DIENE. 6-CHLORO-1-HEXENE AND 8-CHLORO-1-OCTENE. 2-CHLOROPHENYL PHOSPHORODICHLORIDOTHIOATE. 3-CYCLOPENTENE-1-CARBOXYLIC ACID. CYCLOPROPENE: A NEW SIMPLE SYNTHESIS AND ITS DIELS-ALDER REACTION WITH CYCLOPENTADIENE. CYCLOPROPYLACETYLENE. EFFICIENT SYNTHESIS OF BROMIDES FROM CARBOXYLIC ACIDS CONTAINING A SENSITIVE FUNCTIONAL GROUP: DEC-9-ENYL BROMIDE FROM 10-UNDECENOIC ACID. TRIBUTYLSTANNANE (Bu3SnH)-CATALYZED BARTON-McCOMBIE DEOXYGENATION OF ALCOHOLS: 3-DEOXY-1,2:5,6-BIS-O-(1-METHYLETHYLIDENE)-?-D-ribo-HEXOFURANOSE. -30,50-DI-O-BENZOYLTHYMIDINE. PREPARATION OF ENANTIOMERICALLY PURE -N,N-DIBENZYLAMINOALDEHYDES: S-2-(N,N-DIBENZYLAMINO)-3-PHENYLPROPANAL. SYNTHESIS OF SYMMETRICAL trans-STILBENES BY A DOUBLE HECK REACTION OF (ARYLAZO)-AMINES WITH VINYLTRIETHOXYSILANE: trans-4,4'-DIBROMOSTILBENE. PREPARATION AND USE OF N,N'-DI-Boc-N"-TRIFLYLGUANIDINE. SYNTHESIS OF 8,8-DICYANOHEPTAFULVENE FROM CYCLOHEPTATRIENYLIUM TETRAFLUOROBORATE AND BROMOMALONONITRILE. DICYCLOHEXYLBORON TRIFLUOROMETHANESULFONATE. (R,R)-1,2:4,5-DIEPOXYPENTANE. ASYMMETRIC SYNTHESIS OF DIETHYL (R)-(-)-(1-AMINO-3-METHYLBUTYL)PHOSPHONATE. DIETHYL [(PHENYLSULFONYL)METHYL]PHOSPHONATE. 6,7-DIHYDROCYCLOPENTA-1,3-DIOXIN-5(4H)-ONE. SYNTHESIS OF CHIRAL NON-RACEMIC DIOLS FROM (S,S)-1,2,3,4-DIEPOXYBUTANE: (2S,3S)-DIHYDROXY-1,4-DIPHENYLBUTANE. PREPARATION OF (E)-1-DIMETHYLAMINO-3-tert-BUTYLDIMETHYLSILOXY-1,3-BUTADIENE. (2S)-(-)-3-exo-(DIMETHYLAMINO)ISOBORNEOL [(2S)-(-)-DAIB]. 4-DIMETHYLAMINO-N-TRIPHENYLMETHYLPYRIDINIUM CHLORIDE. (R,R)- AND (S,S)-N,N0-DIMETHYL-1,2-DIPHENYLETHYLENE-1,2-DIAMINE. SYNTHESIS OF 1,1-DIMETHYLETHYL (S)-4-FORMYL-2,2-DIMETHYL-3-OXAZOLIDINECARBOXYLATE BY OXIDATION OF THE ALCOHOL. CONVERSION OF NITRILES INTO TERTIARY AMINES: N,N-DIMETHYLHOMOVERATRYLAMINE. NICKEL-CATALYZED COUPLING OF ARYL O-CARBAMATES WITH GRIGNARD REAGENTS: 2,7-DIMETHYLNAPHTHALENE. [4 + 3] CYCLOADDITION IN WATER: 2,4-endo,endo-DIMETHYL-8-OXABICYCLO[3.2.1]OCT-6-EN-3-ONE. SYNTHESIS OF -LACTONES BY ALDOLIZATION OF KETONES WITH PHENYL ESTER ENOLATES: 3,3-DIMETHYL-1-OXASPIRO[3.5]NONAN-2-ONE. ANTI-SELECTIVE BORON-MEDIATED ASYMMETRIC ALDOL REACTION OF CARBOXYLIC ESTERS: (2S, 3R)-2,4-DIMETHYL-1,3-PENTANEDIOL. (4R,5R)-2,2-DIMETHYL- , , ', '-TETRA(NAPHTH-2-YL)-1,3-DIOXOLANE-4,5-DIMETHANOL FROM DIMETHYL TARTRATE AND 2-NAPHTHYLMAGNESIUM BROMIDE. DIMETHYLTITANOCENE. 9,10-DIPHENYLPHENANTHRENE. (R)-2-DIPHENYLPHOSPHINO-20-METHOXY-1,1'-BINAPHTHYL. 5-PHENYLDIPYRROMETHANE AND 5,15-DIPHENYLPORPHYRIN. (4R,5S)-4,5-DIPHENYL-3-VINYL-2-OXAZOLIDINONE. 1S-(-)-1,3-DITHIANE 1-OXIDE. ETHYL (R)-2-AZIDOPROPIONATE. ETHYL 5-CHLORO-3-PHENYLINDOLE-2-CARBOXYLATE. ETHYL 3-(p-CYANOPHENYL)PROPIONATE FROM ETHYL 3-IODOPROPIONATE AND p-CYANOPHENYLZINC BROMIDE. 9-ETHYL-3,6-DIMETHYLCARBAZOLE (DMECZ)*. ETHYL GLYCIDATE FROM (S)-SERINE: ETHYL (R)-(+)-2,3-EPOXYPROPANOATE. (-)-2,4-O-ETHYLIDENE-D-ERYTHROSE AND ETHYL (E)-(-)-4,6-OETHYLIDENE-(4S,5R,1'R)-4,5,6-TRIHYDROXY-2-HEXENOATE. COPPER-CATALYZED CONJUGATE ADDITION OF FUNCTIONALIZED ORGANOZINC REAGENTS TO , ?-UNSATURATED KETONES: ETHYL 5-(3-OXOCYCLOHEXYL)PENTANOATE. ULLMAN METHOXYLATION IN THE PRESENCE OF A 2,5-DIMETHYLPYRROLE-BLOCKED ANILINE: 2-FLUORO-4-METHOXYANILINE. PALLADIUM-CATALYZED AMINATION OF ARYL HALIDES AND ARYL TRIFLATES: N-HEXYL-2-METHYL-4-METHOXYANILINE AND N-METHYL-N-(4-CHLOROPHENYL)ANILINE. 4-HYDROXY[1-13C]BENZOIC ACID. N-HYDROXY-4-(p-CHLOROPHENYL)THIAZOLE-2(3H)-THIONE. [4 + 2] CYCLOADDITION OF 1-DIMETHYLAMINO-3-tert-BUTYLDIMETHYLSILOXY-1,3-BUTADIENE WITH METHYL ACRYLATE: 4-HYDROXYMETHYL-2-CYCLOHEXEN-1-ONE. ASYMMETRIC SYNTHESIS OF (M)-2-HYDROXYMETHYL-1-(2-HYDROXY-4,6-DIMETHYLPHENYL)-NAPHTHALENE VIA A CONFIGURATIONALLY UNSTABLE BIARYL LACTONE. SYNTHESIS AND DIASTEREOSELECTIVE ALKYLATION OF PSEUDOEPHEDRINE AMIDES: (1S,2S)-PSEUDOEPHEDRINEPROPIONAMIDE AND [(1S,2S)-PSEUDOEPHEDRINE-(R)-2-METHYLHYDROCINNAMAMIDE. GENERATION AND USE OF LITHIUM PENTAFLUOROPROPEN-2-OLATE: 4-HYDROXY-1,1,1,3,3- PENTAFLUORO-2-HEXANONE HYDRATE. (R)-(+)-2-HYDROXY-1,2,2-TRIPHENYLETHYL ACETATE. 2-(4-METHOXYPHENYL)-2-CYCLOHEXEN-1-ONE: PREPARATION OF 2-IODO-2-CYCLOHEXEN-1-ONE AND SUZUKI COUPLING WITH 4-METHOXYPHENYLBORONIC ACID. O4,O5-ISOPROPYLIDENE-1,2:3,6-DIANHYDRO-D-GLUCITOL FROM ISOSORBIDE. -MERCAPTOPROPIONITRILE (2-CYANOETHANETHIOL). PREPARATION OF SECONDARY AMINES FROM PRIMARY AMINES VIA 2-NITROBENZENESULFONAMIDES: N-(4-METHOXYBENZYL)-3-PHENYLPROPYLAMINE. 4-METHOXYCARBONYL-2-METHYL-1,3-OXAZOLE. SELECTIVE PROTECTION OF 1,3-DIOLS AT THE MORE HINDERED HYDROXY GROUP: 3-(METHOXYMETHOXY)-1-BUTANOL. (S,E)-1-(METHOXYMETHOXY)-1-TRIBUTYLSTANNYL-2-BUTENE. ACCELERATED SUZUKI COUPLING VIA A LIGANDLESS PALLADIUM CATALYST: 4-METHOXY-20-METHYLBIPHENYL. NUCLEOPHILIC AROMATIC SUBSTITUTION OF ARYL FLUORIDES BY SECONDARY NITRILES: 2-(2-METHOXYPHENYL)-2-METHYLPROPIONITRILE. TRANSFORMATION OF PSEUDOEPHEDRINE AMIDES INTO HIGHLY ENANTIOMERICALLY ENRICHED ALDEHYDES, ALCOHOLS, AND KETONES: (R)- -METHYLBENZENEPROPANAL, (R)- -METHYLBENZENEPROPANOL, AND (R)-2-METHYL-1-PHENYL-3-HEPTANONE. SYNTHESIS OF 4-, 5-, AND 6-METHYL-2,2'-BIPYRIDINE BY A NEGISHI CROSS-COUPLING STRATEGY: 5-METHYL-2,2'-BIPYRIDINE. (1'S,2'S)-METHYL-3O,4O-(1',2'-DIMETHOXYCYCLOHEXANE-10,20 DIYL)- -DMANNOPYRANOSIDE. FORMATION OF -KETO ESTERS FROM -KETO ESTERS: METHYL 5,5-DIMETHYL-4-OXOHEXANOATE. SYNTHESIS OF CHIRAL (E)-CROTYLSILANES: [3R- AND 3S-]-(4E)-METHYL 3-(DIMETHYLPHENYLSILYL)-4-HEXENOATE. IN SITU CATALYTIC EPOXIDATION OF OLEFINS WITH TETRAHYDROTHIOPYRAN-4-ONE AND OXONE: trans-2-METHYL-2,3-DIPHENYLOXIRANE. ALLYLINDATION IN AQUEOUS MEDIA: METHYL 3-(HYDROXYMETHYL)-4-METHYL-2-METHYLENEPENTANOATE. SYNTHESIS OF AMINO ACID ESTER ISOCYANATES: METHYL (S)-2-ISOCYANATO-3-PHENYLPROPANOATE. REDUCTION OF SULFONYL HALIDES WITH ZINC POWDER: S-METHYL METHANETHIOSULFONATE. METHYL CARBAMATE FORMATION VIA MODIFIED HOFMANN REARRANGEMENT REACTIONS: METHYL N-(p-METHOXYPHENYL)CARBAMATE. METHYL 2,3-O-(6,6'-OCTAHYDRO-6,6'-BI-2H-PYRAN-2,2'-DIYL)- -D-GALACTOPYRANOSIDE. [R-(R*,S*)]- -METHYL- -PHENYL-1-PYRROLIDINEETHANOL. METHYL (S)-2-PHTHALIMIDO-4-OXOBUTANOATE. THE SYNTHESIS OF 2-ALKYL-4-PYRONES FROM MELDRUM'S ACID: 2-METHYL-4HPYRAN-4-ONE. CATALYTIC ASYMMETRIC SYNTHESIS OF NITROALDOLS USING A LANTHANUM-LITHIUM-BINOL COMPLEX: (2S,3S)-2-NITRO-5-PHENYL-1,3-PENTANEDIOL. 3-NITROPROPANAL, 3-NITROPROPANOL, AND 3-NITROPROPANAL DIMETHYL ACETAL. [4 + 3] CYCLOADDITION OF AMINOALLYL CATIONS WITH 1,3-DIENES: 11-OXATRICYCLO-[4.3.1.12,5]UNDEC-3-EN-10-ONE. 2-(3-OXOBUTYL)CYCLOPENTANONE-2-CARBOXYLIC ACID ETHYL ESTER. 1-OXO-2-CYCLOHEXENYL-2-CARBONITRILE. PENTA-1,2-DIEN-4-ONE (ACETYLALLENE). ISOMERIZATION OF -ALKYNYL ALLYLIC ALCOHOLS TO FURANS CATALYZED BY SILVER NITRATE ON SILICA GEL: 2-PENTYL-3-METHYL-5-HEPTYLFURAN. (+)-(1S,2R)- AND (-)-(1R,2S)-trans-2-PHENYLCYCLOHEXANOL VIA SHARPLESS ASYMMETRIC DIHYDROXYLATION (AD). (R)-3-PHENYLCYCLOHEXANONE. (2S,3S)-(+)-(3-PHENYLCYCLOPROPYL)METHANOL. MOLYBDENUM CARBONYL-CATALYZED ALKYNOL CYCLOISOMERIZATION: 2-PHENYL-2,3-DIHYDROFURAN. GENERATION OF 1-PROPYNYLLITHIUM FROM (Z/E)-1-BROMO-1-PROPENE: 6-PHENYLHEX-2-YN-5-EN-4-OL. CATALYTIC ASYMMETRIC ALLYLATION REACTIONS: (S)-1-PHENYLMETHOXY)-4-PENTEN-2-OL. CATALYTIC ENANTIOSELECTIVE ADDITION OF DIALKYLZINCS TO ALDEHYDES USING (2S)-(-)-3-exo-(DIMETHYLAMINO)ISOBORNEOL [(2S)-DAIB]: (S)-1-PHENYL-1-PROPANOL. MONO-C-METHYLATION OF ARYLACETONITRILES AND METHYL ARYLACETATES BY DIMETHYL CARBONATE: A GENERAL METHOD FOR THE SYNTHESIS OF PURE 2-ARYLPROPIONIC ACIDS. 2-PHENYLPROPIONIC ACID. PREPARATION OF CYANOALKYNES: 3-PHENYL-2-PROPYNENITRILE. N-VINYLPYRROLIDIN-2-ONE AS A 3-AMINOPROPYL CARBANION EQUIVALENT IN THE SYNTHESIS OF SUBSTITUTED 1-PYRROLINES: 2-PHENYL-1-PYRROLINE. (PHENYL)[2-(TRIMETHYLSILYL)PHENYL]IODONIUM TRIFLATE, AN EFFICIENT AND MILD BENZYNE PRECURSOR: PREPARATION OF 1,4-DIHYDRONAPHTHALENE 1,4-OXIDE. [1.1.1]PROPELLANE. 1,2-METALLATE REARRANGEMENT: (Z)-4-(2-PROPENYL)-3-OCTEN-1-OL. 1,4,7,10-TETRAAZACYCLODODECANE. (+)-(1R,2S,3R)-TETRACARBONYL[(1-3Z)-1-(PHENYLSULFONYL)-BUT-2-EN-1-YL]IRON(1+) TETRAFLUOROBORATE. USE OF 1,2,4,5-TETRABROMOBENZENE AS A 1,4-BENZADIYNE EQUIVALENT: anti- AND syn-1,4,5,8-TETRAHYDROANTHRACENE 1,4:5,8-DIEPOXIDES. INDOLE SYNTHESIS BY Pd-CATALYZED ANNULATION OF KETONES WITH o-IODOANILINE: 1,2,3,4-TETRAHYDROCARBAZOLE. 6A-O-p-TOLUENESULFONYL- -CYCLODEXTRIN. 6A-O-p-TOLUENESULFONYL- -CYCLODEXTRIN. -TOSYLBENZYL ISOCYANIDE. THE DESS-MARTIN PERIODINANE: 1,1,1-TRIACETOXY-1,1-DIHYDRO-1,2-BENZIODOXOL-3-(1H)-ONE. WITTIG OLEFINATION OF PERFLUOROALKYL CARBOXYLIC ESTERS
- SYNTHESIS OF 1,1,1-TRIFLUORO-2-ETHOXY-5-PHENYLPENT-2-ENE AND 1-PERFLUOROALKYL EPOXY ETHERS: 1,1,1-TRIFLUORO-2-ETHOXY-2,3-EPOXY-5-PHENYLPENTANE. 2-TRIMETHYLSILYLETHANESULFONYL CHLORIDE (SES-CI). TRIS(2-PERFLUOROHEXYLETHYL)TIN HYDRIDE: A HIGHLY FLUORINATED TIN HYDRIDE WITH ADVANTAGEOUS FEATURES OF EASY PURIFICATION. VITAMIN D2 FROM ERGOSTEROL. TYPE OF REACTION INDEX. TYPE OF COMPOUND INDEX. FORMULA INDEX. AUTHOR INDEX. GENERAL INDEX. HAZARD AND WASTE DISPOSAL INDEX. CONCORDANCE INDEX.
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collective v. 7 ISBN 9780471515593
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collective v. 8 ISBN 9780471585657
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collective v. 4 ISBN 9780471704706
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collective v. 6 ISBN 9780471852438
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- [The numbers in parentheses refer to the annual volume (in boldface type) and page number where each procedure first appeared] Acylamidoalkyl Acetophenones from Substituted Phenethylamines: 2-(2-Acetamidoethyl)-4,5-dimethoxyacetophenone (56, 3) Thiol Protection with the Acetamidomethyl Group: S-Acetamidomethyl-l-cysteine Hydrochloride (59, 190) Acetic Formic Anhydride (50, 1) Acetone Hydrazone (50, 3) Preparation of Hydrazones: Acetophenone Hydrazone (50, 102) 3 -Acetoxy-5 -cyanocholestan-7-one (52, 100) p-Acetyl- -bromohydrocinnamic Acid (51, 1) , -Dehydrogenation of -Dicarbonyl Compounds by Selenoxide Elimination: 2-Acetyl-2-cyclohexen-1-one (59, 58) 2-Acetyl-1,3-cyclopentanedione (52, 1) 3-Acetyl-2,4-dimethylfuran (53, 1) 2-Acetyl-6-methoxynaphthalene (53, 5) Copper Catalyzed Arylation of -Dicarbonyl Compounds: 2-(1-Acetyl-2-oxopropyl)benzoic Acid (58, 52) 5-Acetyl- 1,2,3,4,5-pentamethylcyclopentadiene (56, 1) 2-Adamantanecarbonitrile (57, 8) Tertiary Alcohols from Hydrocarbons by Ozonation on Silica Gel: 1-Adamantanol (59, 176) Adamantanone (53, 8) Enone Reduction-Enolate Alkylation Sequence: 2-Allyl-3-methylcyclohexanone (56, 52) Preparation of N-Aminoaziridines: trans-1-Amino-2,3-diphenylaziridine, 1-Amino-2-phenylaziridine, and 1-Amino-2-phenylaziridinium Acetate (55, 114) Reduction of Ketones by Use of the Tosylhydrazone Derivatives: Androstan-17 -Ol (52, 122) Aldehydes from 4,4-Dimethyl-2-oxazoline and Grignard Reagents: o-Anisaldehyde (54, 42) [18]Annulene (54, 1) Azetidine (53, 13) Azoethane (52, 11) Diels-Alder Addition of Perchlorobenzyne: Benzobarrelene (59, 71) Benzocyclopropene (55, 12) -Chlorination of Carboxylic Acids Mediated by Chlorosulfonic Acid: -Benzoylamino- -chlorocaproic Acid (59, 20) 1-N-Acylamino-1,3-dienes from 2,4-pentadienoic Acids by the Curtius Rearrangement: Benzyl trans-1,3-Butadiene-1-carbamate (59, 1) Benzyl Chloromethyl Ether (52, 16) 1-Benzylindole (54, 58) N-Alkylindoles from the Alkylation of Sodium Indolide in Hexamethylphosphoric Triamide: 1-Benzylindole (54, 60) 3-Alkylated and 3-Acylated Indoles from a Common Precursor: 3-Benzylindole and 3-Benzoylindole (56, 8) Alkylation of Isoquinolines via 2-Benzoyl-1,2-dihydroisoquinaldonitriles: 1-Benzylisoquinoline (56, 19) The Formation and Alkylation of Specific Enolate Anions from an Unsymmetrical Ketone: 2-Benzyl-2-methylcyclohexanone and 2-Benzyl-6-methylcyclohexanone (52, 39) Sulfide Synthesis: Benzyl Sulfide (58, 138) Bicyclo[1.1.0]butane (51, 55) Boranes in Functionalization of Dienes to Cyclic Ketones: Bicyclo[3.3.1]nonan-9-one (58, 24) Bicyclo[3.2.1]octan-3-one (51, 60) Bicyclo[2.1.0]pent-2-ene (55, 15) Dehydroxylation of Phenols
- Hydrogenolysis of Phenolic Ethers: Biphenyl (51, 82) Controlled-Potential Electrolytic Reduction: 1,1-Bis(bromomethyl)cyclopropane (52, 22) Bis(trifluoromethyl)diazomethane (50, 6) Bis[2,2,2-trifluoro-1-phenyl-1-(trifluoromethyl)ethoxy] Diphenyl Sulfurane (57, 22) Acyloin Condensation in which Chlorotrimethylsilane is Used as a Trapping Agent: 1,2-Bis(trimethylsilyloxy)cyclobutene and 2-Hydroxycyclobutanone (57, 1) 2-Bornene (51, 66) Selective -Bromination of an Aralkyl Ketone with Phenyltrimethylammonium Tribromide: 2-Bromoacetyl-6-methoxynaphthalene and 2,2-Dibromoacetyl-6-methoxynaphthalene (53, 111) Mercury(II) Oxide-Modified Hunsdiecker Reaction: 1-Bromo-3-chlorocyclobutane (51, 106) para-Bromination of Aromatic Amines: 4-Bromo-N,N-dimethyl-3-(trifluoromethyl)aniline (55, 20) Bromohydrins from Alkenes and N-Bromosuccinimide in Dimethyl Sulfoxide
- erythro-2-Bromo-1,2-diphenylethanol (59, 16) Chain Elongation of Alkenes via gem-Dihalocyclopropanes: 2-Bromo-3,3-diphenyl-2-propen-1-yl acetate (56, 32) 2-Bromohexanoyl Chloride (55, 27) 1-Bromo-3-methyl-2-butanone (55, 24) trans, trans-1,3-Butadiene-1,4-diyl Diacetate (50, 24) A New Reagent for tert-Butoxycarbonylation: 2-tert-Butoxycarbonyloxyimino-2-phenylacetonitrile (59, 95) tert-Butoxycarbonyl-l-proline (53, 25) tert-Butyl Azidoformate (50, 9
- 57, 122) tert-Butylcyanoketene (55, 32) cis-4-tert-Butylcyclohexanol (50, 13) Polymeric Carbodiimide. Moffat Oxidation: 4-tert-Butylcyclohexanone (56, 99) Oxidation of Alcohols by Methyl Sulfide- N-Chlorosuccinimide- Triethylamine: 4-tert-Butylcyclohexanone (58, 122) 2-tert-Butyl-1,3-diaminopropane (53, 21) Photochemical Ring-Contraction of 2-Ethoxypyrrolin-5-ones to Cyclopropanone Derivatives: tert-Butyl N-(1-Ethoxycyclopropyl)carbamate (59, 132) Phase-Transfer Hofmann Carbylamine Reaction: tert-Butyl Isocyanide (55, 96) Sulfide Synthesis in Preparation of Unsymmetrical Dlalkyl Disulfides: sec-Butyl Isopropyl Disulfide (58, 147) 3-Butyl-2-Methylhept-1-en-3-ol (52, 19) Monoalkylation of , -Unsaturated Ketones via Metalloenamines: 1-Butyl-10-methyl- 1(9)-2-octalone (57, 69) -Diketones from Methyl Alkyl Ketones: 3-n-Butyl-2,4-pentanedione (51, 90) Secondary and Tertiary Alkyl Ketones from Carboxylic Acid Chlorides and Lithium Phenylthio(alkyl)cuprate Reagents: tert-Butyl Phenyl Ketone (55, 122) Removal of N -Benzyloxycarbonyl Groups from Sulfur-Containing Peptides by Catalytic Hydrogenation in Liquid ammonia: O-tert-Butyl-L-seryl-S-tert-butyl-l-cysteine tert-Butyl Ester (59, 159) Esterification of Hindered Alcohols: tert-Butyl p-Toluate (51, 96) Peptide Syntheses Using N-Ethyl-5-phenylisoxazolium-3'-sulfonate: Carbobenzoxy-L-asparaginyl-L-leucine Methyl Ester and N-Carbobenzoxy-3-hydroxy-L-prolylglycylglycine Ethyl Ester (56, 88) Carbonyl Cyanide (51, 70) 3-Chlorocyclobutanecarboxylic Acid (51, 73) (z)-4-Chloro-4-hexenyl Trifluoroacetate (57, 26) m-Chloroperbenzoic Acid (50, 15) 3-(4-Chlorophenyl)-5-(4-Methoxyphenyl)Isoxazole (55, 39) -Chloro Enamines, Reactive Intermediates for Synthesis: 1-Chloro-N,N,2-trimethylpropenylamine (59, 26) Modified Clemmensen Reduction: Cholestane (53, 86) Conjugate Reduction of , -Unsaturated p-Toluenesulfonylhydrazones to Alkenes with Catecholborane: 5 -Cholest-3-ene (59, 42) 5 -Cholest-3-Ene-5-Acetaldehyde (54, 71) 18-Crown-6 (57, 30) Cinnamonitrile (50, 18) Preparation of Cyano Compounds Using Alkylaluminum Intermediates: 1-Cyano-6-methoxy-3,4-Dihydronaphthalene (52, 96) Cyclobutadieneiron Tricarbonyl (50, 21) Aldehydes from acid Chlorides by Reduction of Ester-mesylates with Sodium Borohydride: Cyclobutanecarboxaldehyde (51, 11) Cyclic Ketones from 1,3-Dithiane: Cyclobutanone (51, 76) Cyclobutanone from Methylenecyclopropane via Oxaspiropentane (57, 36) Cyclobutanone Via Solvolytic Cyclization (54, 84) One-carbon Ring Expansion of Cycloalkanones to Conjugated Cycloalkenones: 2-Cyclohepten-1-one (59, 113) Nitriles from Ketones: Cyclohexanecarbonitrile (58, 101) Aldehydes from Olefins: Cyclohexanecarboxaldehyde (57, 11) Catalytic Osmium Tetroxide Oxidation of Olefins: cis-1,2-Cyclohexanediol (58, 43) Stereoselective Hydroxylation with Thallium(i) Acetate and Iodine: trans- and cis-1,2-Cyclohexanediols (59, 169) Cleavage of Methyl Ethers with Iodotrimethylsilane: Cyclohexanol from Cyclohexyl Methyl Ether (59, 35) Preparation of , -Unsaturated Aldehydes via the Wittig Reaction: Cyclohexylideneacetaldehyde (53, 104) Cyclopropenone (57, 41) Cyclopropyldiphenylsulfonium Tetrafluoroborate (54, 27) Ring Contraction via a Favorskii-Type Rearrangement: Cycloundecanone (56, 107) Hydrogenation of Aromatic Nuclei: 1-Decalol (51, 103) Oxidation with the Chromium Trioxide-Pyridine Complex Prepared in situ: 1-Decanal (55, 84) Reduction of Alkyl Halides and Tosylates with Sodium Cyanoborohydride in Hexamethylphosphoric Triamide (HMPA): A. 1-Iododecane to n-Decane B. 1-Dodecyl Tosylate to n-Dodecane (53, 107) Diamantane: Pentacyclo[7.3.1.14,12.02,7.06,11]tetradecane (53, 30) Macrocyclic Diimines: 1,10-dlazacycloeCtadecane (54, 88) Dlazoacetophenone (53, 35) 2-diazocycloalkanones: 2-diazocyclohexanone (51, 86) 2-diazopropane (50, 27) Macrocyclic Polyethers: Dibenzo-18-crown-6 Polyether and Dicyclohexyl-18-crown-6 Polyether (52, 66) 1,2-Diaroylcyclopropanes: trans-1,2-Dibenzoylcyclopropane (52, 33) ,???-Dibromodibenzyl Sulfone (50, 31) Phosphine-Nickel Complex Catalyzed Cross-Coupling of Grignard Reagents with Aryl and Alkenyl Halides: 1,2-Dibutylbenzene (58, 127) Oxidation with Bis(Salicylidene)ethylenediiminocobalt(II) (Salcomine)
- 2,6-Di-tert-butyl-p-benzoquinone (57, 78) Diazo Transfer by Means of Phase-transfer Catalysis: Di-tert-Butyl Diazomalonate (59, 66) Di-tert-butyl Dicarbonate (57, 45) cis-3,4-Dichlorocyclobutene (50, 36) cis-Dichloroalkanes from Epoxides: cis-1,2-Dichlorocyclohexane (58, 64) 2,3-Dicyanobutadiene as a Reactive Intermediate by in situ Generation from 1,2-Dicyanocyclobutene: 2,3-Dicyano-1,4,4a,9a-tetrahydrofluorene (58, 67) Dideuteriodiazomethane (53, 38) Diethylaluminum cyanide (52, 90) Diethylaminosulfur trifluoride (57, 50) Diethyl tert-Butylmalonate (50, 38) 2-Trimethylsilyloxy-1,3-butadiene as a Reactive Diene: Diethyl trans-4-Trimethylsilyloxy-4-cyclohexene-1,2-dicarboxylate (58, 163) Diethyl 2-(Cyclohexylamino)vinylphosphonate (53, 44) Radical Anion Arylation: Diethyl Phenylphosphonate (58, 134) Diethyl trans- 4-Tetrahydrophthalate (50, 43) Homogeneous Catalytic Hydrogenation: Dihydrocarvone (53, 63) trans-1,2-Dihydrophthalic Acid (50, 50) 5,6-Dihydro-2H-pyran-2-one and 2H-Pyran-2-One (56, 49) 2,4-Dimethoxybenzonitrile (50, 52) Biaryls from Simple Arenes via Organotellurium Intermediates
- 4,4'-Dimethoxy-1,1'-Biphenyl (57, 18) 6,7-Dimethoxy-3-Isochromanone (55, 45) Regioselective Mannich Condensation with Dimethyl(methylene)ammonium Trifluoroacetate: 1-Dimethylamino-4-methyl-3-pentanone (59, 153) Directed Lithiation of Aromatic Compounds: (2-Dimethylamino-5-methylphenyl)diphenylcarbinol (53, 56) Use of Dipotassium Nitrosodisulfonate (fremy's Salt): 4,5-Dimethyl-o-Benzoquinone (52, 88) 1,2-Dimethylcyclobutenes by Reductive Ring-Contraction of Sulfolanes: cis-7,8-Dimethylbicyclo[4.2.0]oct-7-Ene (57, 53) 4,4'-Dimethyl-1,1'-biphenyl (55, 48) N,N-Dimethyl-5 -cholest-3-Ene-5-acetamide (54, 77) Conversion of Esters to Amides with Dimethylaluminum Amides: N,N-Dimethylcyclohexanecarboxamide (59, 49) 4,4-Dimethyl-2-Cyclohexen-1-one (53, 48) Reductive Amination with Sodium Cyanoborohydride: N,N- Dimethylcyclohexylamine (52, 124) N,N-Dimethyldodecylamine Oxide (50, 56) Dimethyl Nitrosuccinate (57, 60) Dimethyl 2,3-Pentadienedioate (57, 62) Allylically Transposed Amines from Allylic Alcohols
- 3,7-Dimethyl-1,6-octadien-3-amine (58, 4) Bicyclic Ketones for The Synthesis of Tropinoids: 2 ,4 -Dimethyl-8-oxabicyclo[3.2.1]oct-6-en-3-one (58, 17) 2,2-Dimethyl-4-Phenylbutyric Acid (50, 58) Cyclopentenones from , '-Dibromoketones and Enamines: 2,5-Dimethyl-3-phenyl-2-cyclopenten-1-one (58, 56) Alkylations of Aldehydes via Reaction of the Magnesioenamine Salt of an Aldehyde: 2,2-Dimethyl-3-phenylpropionaldehyde (54, 46) 3,5-Dinitrobenzaldehyde (53, 52) 2,3-Diphenyl-1,3-butadiene (50, 62) Reagents for Synthesis of Organoselenium Compounds: Diphenyl Diselenide and Benzeneselenenyl Chloride (59, 141) Aromatic Hydrocarbons from Aromatic Ketones and Aldehydes: 1,1-Diphenylethane (55, 7) Nucleophilic -sec-Aminoalkylation: 2-(Diphenylhydroxymethyl)pyrrolidine (58, 113) Diphenylketene (52, 36) Alkenes via Hofmann Elimination: Use of Ion-Exchange Resin for Preparation of Quaternary Ammonium Hydroxides: Diphenylmethyl Vinyl Ether (55, 3) 2,3-Diphenylvinylene Sulfone (50, 65) 1,3-Dithiane (50, 72) 2,2'-Dithienyl Sulfide (50, 75) Selective Epoxidation of Terminal Double Bonds: 10, 11-Epoxyfarnesyl Acetate (56, 112) 1-Ethoxy-1-butyne (57, 65) Demethylation of Methyl Aryl Ethers: 4-Ethoxy-3-hydroxybenzaldehyde (56, 44) Carbine Generation by -Elimination with Lithium 2,2,6,6-Tetramethylpiperidide: 1-Ethoxy-2-p-tolylcyclopropane (58, 37) Esterification of Carboxylic Acids with Trialkyloxonium Salts
- Ethyl and Methyl 4-Acetoxybenzoates (56, 59) ortho-Alkylation of Anilines: Ethyl 4-Amino-3-Methylbenzoate (56, 15) Ethyl 5 -Cholest-3-ene-5-acetate (54, 74) Free-Radical Cyclization: Ethyl 1-Cyano-2-Methylcyclohexanecarboxylate (55, 57) 2,2-(Ethylenedithio)cyclohexanone (54, 37) A General Synthesis of 4-Isoxazolecarboxylic Esters: Ethyl 3-Ethyl-5-methyl-4-isoxazolecarboxylate (53, 59) 3-Alkyl-1-alkynes Synthesis: 3-Ethyl-1-hexyne (58, 1) -Hydroxy Esters from Ethyl Acetate and Aldehydes or Ketones: Ethyl 1-Hydroxycyclohexylacetate (53, 66) Indoles from Anilines: Ethyl 2-Methylindole-5-carboxylate (56, 72) Stereoselective Synthesis of Trisubstituted Olefins: Ethyl 4-Methyl-(E)-4,8-nonadienoate (53, 116) Metalation of 2-Methylpyridine Derivatives: Ethyl 6-Methylpyridine-2-acetate (52, 75) Ethyl 1-Naphthylacetate (50, 77) Ethyl (E)-3-Nitroacrylate [Replaced by Methyl (E)-3-Nitroacrylate] (56, 65
- replaced) -Ketoesters from Aldehydes via Diethyl Acylsuccinates: Ethyl 4-oxohexanoate (58, 79) Ethyl Pyrrole-2-Carboxylate (51, 100) Thiazoles from Ethyl Isocyanoacetate and Thiono Esters: Ethyl Thiazole-4-carboxylate (59, 183) Carboxylation of Aromatic Compounds: Ferrocenecarboxylic Acid (56, 28) Fluorinations with Pyridinium Polyhydrogen Fluoride Reagent: 1-Fluoroadamantane (58, 75) Aldehydes from Aromatic Nitriles: 4-Formylbenzenesulfonamide (51, 20) Geranyl Chloride (54, 63) Allylic Chlorides from Allylic Alcohols: Geranyl Chloride (54, 68) Glutaconaldehyde Sodium Salt From Hydrolysis of Pyridinium-1-sulfonate (59, 79) Aldehydes from Primary Alcohols by Oxidation with Chromium Trioxide: Heptanal (52, 5) Conversion of Nitro to Carbonyl by Ozonolysis of Nitronates: 2,5-Heptanedione (56, 36) Macrocyclic Polyamines: 1,4,7,10,13,16-Hexaazacyclooectadecane (58, 86) Cuprous Ion-Catalyzed Oxidative Cleavage of Aromatic o-Diamines by Oxygen:(Z,Z)-2,4-Hexadienedinitrile (57, 33) Hexafluoroacetone Imine (50, 81) 3-Trimethylsilyl-3-buten-2-one as Michael Acceptor for Conjugate Addition-Annelation: cis-4,4a,5,6,7,8-Hexahydro-4a,5-dimethyl-2(3H)-naphthalenone (58, 158) Nitrones for Intramolecular 1,3-Dipolar Cycloadditions: Hexahydro-1,3,3,6-tetramethyl-2,1-benzisoxazoline (58, 106) (E)-4-Hexen-1-ol (55, 62) Fragmentation of , -Epoxyketones to Acetylenic Aldehydes and Ketones: Preparation of 2,3-Epoxycyclohexanone and its Fragmentation to 5-Hexynal (55, 52) -Hydroxy- , -Unsaturated Aldehydes via 1,3-Bis(methylthio)allyllithium: trans-4-Hydroxy-2-hexenal (54, 19) 17 -Hydroxy-5-oxo-3,5-seco-4-norandrostane-3-carboxylic Acid (55, 67) Directed Aldol Condensations: threo-4-Hydroxy-3-phenyl-2-heptanone (54, 49) Macrolides from Cyclization of -Bromocarboxylic Acids: 11-Hydroxyundecanoic Lactone (58, 98) Direct Iodination of Polyalkylbenzenes: Iododurene (51, 94) trans-Iodopropenylation of Alkyl Halides: (E)-1-Iodo-4-phenyl-2-butene (56, 77) 2-Iodo-p-xylene (55, 70) cis- , -Unsaturated Acids: Isocrotonic Acid (53, 123) Trichloromethyl Chloroformate as a Phosgene Equivalent: 3-Isocyanatopropanoyl Chloride (59, 195) Hydroboration of Olefins: (+)-Isopinocampheol [Replaced by ( )-Isopinocampheol] (52, 59) ( )-Isopinocampheol (New) Reaction of Aryl Halides with -Allylnickel Halides: Methallylbenzene (52, 115) Sulfonyl Cyanides: Methanesulfonyl Cyanide (57, 88) 1,6-Methano[10]annulene (54, 11) Vinyl Sulfides from Thioacetals with Copper(I) Trifluoromethanesulfonate: (Z)-2-Methoxy-1-phenylthio-1,3-butadiene (59, 202) 6-Methoxy- -tetralone (51, 109) Methyl Groups by Reduction of Aromatic Carboxylic Acids with Trichlorosilane-tri-n-propylamine: 2-Methylbiphenyl (56, 83) 1-d-Aldehydes from Organometallic Reagents: 2-Methylbutanal-1-d (51, 31) Preparation of Vinyl Trifluoromethanesulfonates: 3-methyl-2-buten-2-yl Triflate (54, 79) Preparation and Reductive Cleavage of Enol Phosphates: 5-Methylcoprost-3-Ene (52, 109) Oxymercuration-Reduction: Alcohols from Olefins: 1-Methylcyclohexanol (53, 94) Reductive Cleavage of Allylic Alcohols, Ethers, or Acetates to Olefins: 3-Methylcyclohexene (56, 101) -Ketoesters to Prepare Cyclic Diketones: 2-Methyl-1,3-cyclopentanedione (58, 83) Sulfide Contraction via Alkylative Coupling: 3-Methyl-2,4-Heptanedione (55, 127) Isoxazole Annelation Reaction: 1-Methyl-4,4a,5,6,7,8-Hexahydronaphthalen-2(3H)-one (53, 70) Addition of Organolithium Reagents to Allyl Alcohol: 2-Methyl-1-Hexanol (55, 1) Conversion of Primary Alcohols to Urethanes via the Inner Salt of Methyl (carboxysulfamoyl)Triethylammonium Hydroxide: Methyl n-Hexylcarbamate (56, 40) Methyl 2-Alkynoates from 3-Alkyl-2-pyrazolin-5-ones: Methyl 2-Hexynoate (55, 73) Methyl (trans-2-Iodo-1-Tetralin)carbamate (51, 112) Methyl Nitroacetate (55, 77) Methyl (E)-3-Nitroacrylate (New) 2-Methyl-2-nitrosopropane and Its Dimer (52, 77) Nucleophilic Acylation with Disodium Tetracarbonylferrate: Methyl 7-Oxoheptanoate and Methyl 7-Oxooectanoate (59, 102) Aldehydes from Allylic Alcohols and Phenylpalladium Acetate: 2-Methyl-3-phenylpropionalde (51, 17) Endocyclic Enamine Synthesis: N-Methyl-2-phenyl- 2-tetrahydropyridine (54, 93) Hydrogenolysis of Carbon-Halogen Bonds with Chromium(II)-en Perchlorate: Naphthalene from 1-Bromonaphthalene (52, 62) Thiophenols from Phenols: 2-Naphthalenethiol (51, 139) S(-)- -(1-Naphthyl)ethylamine (55, 80) Alkyl Iodides: Neopentyl Iodide and Iodocyclohexane (51, 44) Sulfide Synthesis in Preparation of Dialkyl and Alkyl Aryl Sulfides: Neopentyl Phenyl Sulfide (58, 143) 4-Nitrobenzyl Fluoride (57, 72) 1-Nitrocyclooectene (50, 84) Formation and Photochemical Wolff Rearrangement of Cyclic -Diazo Ketones: D-Norandrost-5-en-3 -ol-16-carboxylic Acids (52, 53) Highly Reactive Magnesium for the Preparation of Griignard Reagents: 1-Norbornanecarboxylic Acid (59, 85) 9,10-Octalin (50, 88) 2,2,7,7,12,12,17,17-Octamethyl-21,22,23,24-tetraoxaperhydroquaterene (57, 74) Orcinol Monomethyl Ether (53, 90) 1,6-Oxido[10]annulene (55, 86) Cyanide-Catalyzed Conjugate Addition of Aryl Aldehydes: 4-Oxo-4-(3-pyridyl)butyronitrile (59, 53) Aldehydes from sym-Trithlane: n-Pentadecanal (51, 39) (Pentafluorophenyl)acetonitrile (57, 80) Pentafluorophenylcopper Tetramer, a Reagent for Synthesis of Fluorinated Aromatic Compounds (59, 122) trans-3-Penten-2-one (51, 115) Arene Oxide Synthesis: Phenanthrene-9,10-oxide (58, 12) Free-Radical Alkylation of Quinones: 2-Phenoxymethyl-1,4-Benzoquinone (56, 68) 3-Phenyl-2H-azirine-2-carboxaldehyde (57, 83) Phase-Transfer Alkylation of Nitriles: 2-Phenylbutyronitrile (55, 91) Directed Aldol Condensations: - Phenylcinnamaldehyde (50, 66) Aldehydes from 2-Benzyl-4,4,6-Trimethyl-5,6-dihydro-1,3(4H)-oxazine: 1-Phenylcyclopentanecarboxaldehyde (51, 24) Amines from Mixed Carboxylic-Carbonic Anhydrides: 1-Phenylcyclopentylamine (51, 48) cis-2-Phenylcyclofropanecarboxylic Acid (50, 94) Substitution of Aryl Halides with Copper(i) Acetylides: 2-Phenylfuro[3,2-b]pyridine (52, 128) Ketones and Alcohols from Organoboranes: Phenyl Heptyl Ketone, 1-Hexanol, and 1-Octanol (53, 77) 1-Phenyl-1,4-pentadiyne and 1-Phenyl-1,3-pentadiyne (50, 97) Phenylation with Diphenyliodonium Chloride
- 1-Phenyl-2,4-pentanedione (51, 128) 1-Phenyl-4-phosphorinanone (53, 98) 4-Phenyl-1,2,4-triazoline-3,5-dione (51, 121) 2-Phenyl-2-vinylbutyronitrile (55, 99) Boranes in Functionalization of Olefins to Amines: 3-Pinanamine (58, 32) Allylic Oxidation with Hydrogen Peroxide-Selenium Dioxide: trans-Pinocarveol (56, 25) Base-Induced Rearrangement of Epoxides to Allylic Alcohols: trans-Pinocarveol (53, 17) Polymeric Carbodiimide. Preparation (56, 95) Alkynes via Phase Transfer Catalyzed Dehydrohalogenation: Propiolaldehyde Diethyl Acetal (59, 10) Rearrangement of Bridgehead Alcohols to Polycyclic Ketones by Fragmentation-Cyclization: 4-Protoadamantanone (Tricyclo[4.3.1.03.8]Decan-4-One) (59, 147) Quadricyclane (51, 133) 1,2,3,4-Tetrahydro- -Carboline (51, 136) Aziridines from -Iodocarbamates: 1,2,3,4-Tetrahydronaphthalene(1,2)Imine (51, 53) 2,3,4,5-Tetrahydropyridine Trimer (56, 118) 3,3,6,6-Tetramethoxy-1,4-Cyclohexadiene (57, 92) 2,2,3,3-Tetramethyliodocyclopropane (52, 132) 4H-1,4-Thiazine l,1-Dioxide (52, 135) 2-Thiophenethiol (50, 104) p-Tolylsulfonyldiazomethane (57, 95) p-Tolylsulfonylmethyl Isocyanide (57, 102) Tri-tert-Butylcyclopropenyl Tetrafluoroborate (54, 97) Tricarbonyl[2,3,4,5- )-2,4,-Cyclohexadien-1-One]Iron and Tricarbonyl[(1,2,3,4,5- )-2-Methyoxy-2,4-Cyclohexadien-1-Yl]Iron(1+) Hexafluorophosphate(1 ) from Anisole (57, 107) Alkylation of Dimedone with a Tricarbonyl(diene)Iron Complex: Tricarbonyl[2-[2,3,4,5- )-4-Methoxy-2,4-Cyclohexadien-1-yl]-5,5-Dimethyl-1,3-Cyclohexanedione]iron (57, 16) Cyclobutadiene in Synthesis: endo-Tricyclo[4.4.0.02,5]Deca-3,8-Diene-7,10-Dione (55, 43) Trifluoroacetylation of Amines and Amino Acids Under Neutral, Mild Conditions: N-Trifluoroacetanilide and N-Trifluoroacetyl-L-Tyrosine (56, 122) Aldehydes from Acid Chlorides by Modified Rosenmund Reduction: 3,4,5-Trimethoxybenzaldehyde (51, 8) Oxidation with the Nitrosodisulfonate Radical. I. Preparation and Use of Disodium Nitrosodisulfonate: Trimethyl-p-Benzoquinone (52, 83) 2,2-(Trimethylenedithio)Cyclohexanone (54, 39) Trimethylene Dithiotosylate and Ethylene Dithiotosylate (54, 33) Trimethyloxonium Tetrafluoroborate (51, 142) 3,5,5-Trimethyl-2-(2-Oxopropyl)-2-Cyclohexen-1-One (57, 113) Aldehydes by Oxidation of Terminal Olefins with Chromyl Chloride: 2,4,4-Trimethylpentanal (51, 4) Trimethylsilyl Azide (50, 107) 3-Trimethylsilyl-3-Buten-2-One: a Michael Acceptor (58, 152) Tropolone (57, 117) Preparation of Alkenes by Reaction of Lithium Dipropenylcuprates with Alkyl Halides: (E)-2-Undecene (55, 103
- deleted) General Index Frmula Index Hazard Index Author Index Concordance Index
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collective v. 12 ISBN 9781118117828
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Table of Contents
by "Nielsen BookData"